6-bromo-2-naphthylbenzoate

Base Information

Chemical Name:6-bromo-2-naphthylbenzoate
CAS No.:74634-34-7
Molecular Formula:C₁₇H₁₁BrO₂
Molecular Weight:327.177
Hs Code.:
Mol file:74634-34-7.mol

Synonyms:

Suppliers and Price of 6-bromo-2-naphthylbenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-bromo-2-naphthylbenzoate

Chemical Property:

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Technology Process of 6-bromo-2-naphthylbenzoate

There total 6 articles about 6-bromo-2-naphthylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 15231-91-1
6-bromo-naphthalen-2-ol

: 591-50-4
iodobenzene

: 50978-45-5
3-oxobenzo[d]isothiazole-2(3H)-carbaldehyde 1,1-dioxide

: 74634-34-7
6-bromonaphthalen-2-yl benzoate

Guidance literature:: With palladium 10% on activated carbon; sodium carbonate; at 80 ℃; for 18h; Green chemistry;
DOI:10.1039/c6gc03027k

Reference yield:

: 15231-91-1
6-bromo-naphthalen-2-ol

: N′-benzoyl-N,N′-dimethoxybenzohydrazide

: 74634-34-7
6-bromonaphthalen-2-yl benzoate

Guidance literature:: With zinc trifluoromethanesulfonate; potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 21h;
DOI:10.1002/adsc.201701646

Reference yield:

: 2446-51-7
N-methoxybenzamide

: 74634-34-7
6-bromonaphthalen-2-yl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 3.5 h / 0 °C / Electrolysis

2: zinc trifluoromethanesulfonate; potassium carbonate / N,N-dimethyl-formamide / 21 h / 20 °C

With tetra-(n-butyl)ammonium iodide; zinc trifluoromethanesulfonate; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1002/adsc.201701646