acetal-aminal of α-phenyl-β-dimethylaminoacrolein

Base Information

• Chemical Name: acetal-aminal of α-phenyl-β-dimethylaminoacrolein
• CAS No.: 74869-78-6
• Molecular Formula: C₁₄H₂₂N₂O
• Molecular Weight: 234.341
• Mol file: 74869-78-6.mol

Synonyms:

Chemical Property of acetal-aminal of α-phenyl-β-dimethylaminoacrolein

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acetal-aminal of α-phenyl-β-dimethylaminoacrolein

There total 4 articles about acetal-aminal of α-phenyl-β-dimethylaminoacrolein which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

potassium methanolate (865-33-8) + ((Z)-3-Dimethylamino-2-phenyl-allylidene)-dimethyl-ammonium; perchlorate (7089-34-1) → acetal-aminal of α-phenyl-β-dimethylaminoacrolein (74869-78-6)

Guidance literature:

In benzene; for 2h; Heating;

DOI:10.1007/BF00949683

Reference yield:

potassium methanolate (865-33-8) + ((Z)-3-Dimethylamino-2-phenyl-allylidene)-dimethyl-ammonium; perchlorate (7089-34-1) → acetal-aminal of α-phenyl-β-dimethylaminoacrolein (74869-78-6) + C15H25N3 (116547-68-3)

Guidance literature:

With dimethyl amine; at 75 - 78 ℃; for 2h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1007/BF00962665

Reference yield:

((Z)-3-Dimethylamino-2-phenyl-allylidene)-dimethyl-ammonium; perchlorate (7089-34-1) + dimethyl amine (124-40-3) → acetal-aminal of α-phenyl-β-dimethylaminoacrolein (74869-78-6) + C15H25N3 (116547-68-3)

Guidance literature:

With potassium methanolate; at 75 - 78 ℃; for 2h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1007/BF00962665

upstream raw materials:

potassium methanolate

((Z)-3-Dimethylamino-2-phenyl-allylidene)-dimethyl-ammonium; perchlorate

dimethyl amine

phenylacetic acid

Downstream raw materials:

2-(3-dimethylamino-2-phenylprop-2-enylidene)benzothiophene-3(2H)-one

3-[(Z)-3-Dimethylamino-2-phenyl-prop-2-en-(Z)-ylidene]-1-methyl-1,3-dihydro-indol-2-one

(E)-2,6-Dicyano-4-phenyl-hepta-2,4-dienedinitrile

1-methyl-3-phenyl-1H-pyrrole