2-(4'-isopropoxy-3'-methoxy-5'-methylphenyl)-4,4-dimethyl-2-oxazoline

Base Information

Chemical Name:2-(4'-isopropoxy-3'-methoxy-5'-methylphenyl)-4,4-dimethyl-2-oxazoline
CAS No.:101417-39-4
Molecular Formula:C₁₆H₂₃NO₃
Molecular Weight:277.364
Hs Code.:

Synonyms:

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Chemical Property of 2-(4'-isopropoxy-3'-methoxy-5'-methylphenyl)-4,4-dimethyl-2-oxazoline

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Technology Process of 2-(4'-isopropoxy-3'-methoxy-5'-methylphenyl)-4,4-dimethyl-2-oxazoline

There total 8 articles about 2-(4'-isopropoxy-3'-methoxy-5'-methylphenyl)-4,4-dimethyl-2-oxazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 101417-38-3
N-(2'-hydroxy-1',1'-dimethylethyl)-4-isopropoxy-3-methoxy-5-methylbenzamide

: 101417-39-4
2-(4'-isopropoxy-3'-methoxy-5'-methylphenyl)-4,4-dimethyl-2-oxazoline

Guidance literature:: With thionyl chloride; for 0.05h;

Reference yield:

: 5034-74-2
5-bromo-3-methoxysalicylaldehyde

: 101417-39-4
2-(4'-isopropoxy-3'-methoxy-5'-methylphenyl)-4,4-dimethyl-2-oxazoline

Guidance literature:: Multi-step reaction with 7 steps

1: 80 percent / anhydrous potassium carbonate, potassium iodide / dimethylformamide / 15 h / 50 °C

2: 1.)hydrazine hydrate 2.)potassium hydroxide / 1.) diethylene glycol, 100 deg C, 0.5 h, 2.) reflux, 1.5 h

3: 87 percent / N,N-dimethylformamide / 2 h / Heating

4: 85 percent / sodium hydroxide / methanol; H₂O / 72 h / Heating

5: 90 percent / thionyl chloride / 24 h / Ambient temperature

6: 90 percent / CH₂Cl₂ / 2.5 h / Ambient temperature

7: 90 percent / thionyl chloride / 0.05 h

With potassium hydroxide; sodium hydroxide; thionyl chloride; potassium carbonate; hydrazine hydrate; N,N-dimethyl-formamide; potassium iodide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 101417-39-4
2-(4'-isopropoxy-3'-methoxy-5'-methylphenyl)-4,4-dimethyl-2-oxazoline

Guidance literature:: Multi-step reaction with 8 steps

1: 82 percent / bromine / acetic acid / 0.08 h / 10 - 15 °C

2: 80 percent / anhydrous potassium carbonate, potassium iodide / dimethylformamide / 15 h / 50 °C

3: 1.)hydrazine hydrate 2.)potassium hydroxide / 1.) diethylene glycol, 100 deg C, 0.5 h, 2.) reflux, 1.5 h

4: 87 percent / N,N-dimethylformamide / 2 h / Heating

5: 85 percent / sodium hydroxide / methanol; H₂O / 72 h / Heating

6: 90 percent / thionyl chloride / 24 h / Ambient temperature

7: 90 percent / CH₂Cl₂ / 2.5 h / Ambient temperature

8: 90 percent / thionyl chloride / 0.05 h

With potassium hydroxide; sodium hydroxide; thionyl chloride; bromine; potassium carbonate; hydrazine hydrate; N,N-dimethyl-formamide; potassium iodide; In methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;