p-Tolylazobenzyliden-4-biphenylamin

Base Information

• Chemical Name: p-Tolylazobenzyliden-4-biphenylamin
• CAS No.: 32478-78-7
• Molecular Formula: C₂₆H₂₁N₃
• Molecular Weight: 375.473
• Mol file: 32478-78-7.mol

Synonyms:

Chemical Property of p-Tolylazobenzyliden-4-biphenylamin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of p-Tolylazobenzyliden-4-biphenylamin

There total 3 articles about p-Tolylazobenzyliden-4-biphenylamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-4-nitrosobenzene (623-11-0) → p-Tolylazobenzyliden-4-biphenylamin (32478-78-7)

Guidance literature:

Multi-step reaction with 2 steps

1: AcOH / methanol

2: (i) (hydrolysis), (ii) /BRN= 386533/, AcOH

With acetic acid; In methanol;

DOI:10.1021/jo00967a004

Reference yield:

N-(p-aminobenzyl)acetamide (99362-10-4) → p-Tolylazobenzyliden-4-biphenylamin (32478-78-7)

Guidance literature:

Multi-step reaction with 2 steps

1: AcOH / methanol

2: (i) (hydrolysis), (ii) /BRN= 386533/, AcOH

With acetic acid; In methanol;

DOI:10.1021/jo00967a004

Reference yield:

N-acetamid (32479-21-3) + 4-phenylalanine (92-67-1) → p-Tolylazobenzyliden-4-biphenylamin (32478-78-7)

Guidance literature:

Multistep reaction; (i) (hydrolysis), (ii) /BRN= 386533/, AcOH;

DOI:10.1021/jo00967a004

upstream raw materials:

N-acetamid

4-phenylalanine

1-methyl-4-nitrosobenzene

N-(p-aminobenzyl)acetamide