Technology Process of 2-(4'-isopropoxy-3'-methoxyphenyl)-6,7-methylenedioxy-3,4-dihydronaphtalen-1(2H)-one
There total 7 articles about 2-(4'-isopropoxy-3'-methoxyphenyl)-6,7-methylenedioxy-3,4-dihydronaphtalen-1(2H)-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; trichlorophosphate;
In
acetonitrile;
at 55 - 60 ℃;
for 3h;
Product distribution;
Mechanism;
different solvents and conditions;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydroxide 10percent / ethanol / 14 h / Ambient temperature
2: acetic acid / 2-ethoxy-ethanol; H2O / 0.13 h / 120 °C
3: sodium hydroxide / ethanol; H2O / 5 h / Heating
4: H2 / palladium chloride, charcoal / acetic acid; H2O / Ambient temperature
5: 91.3 percent / phosphoryl trichloride, potassium carbonate / acetonitrile / 3 h / 55 - 60 °C / different solvents and conditions
With
sodium hydroxide; hydrogen; potassium carbonate; acetic acid; trichlorophosphate;
pyrographite; palladium dichloride;
In
2-ethoxy-ethanol; ethanol; water; acetic acid; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydroxide 10percent / ethanol / 14 h / Ambient temperature
2: acetic acid / 2-ethoxy-ethanol; H2O / 0.13 h / 120 °C
3: sodium hydroxide / ethanol; H2O / 5 h / Heating
4: H2 / palladium chloride, charcoal / acetic acid; H2O / Ambient temperature
5: 91.3 percent / phosphoryl trichloride, potassium carbonate / acetonitrile / 3 h / 55 - 60 °C / different solvents and conditions
With
sodium hydroxide; hydrogen; potassium carbonate; acetic acid; trichlorophosphate;
pyrographite; palladium dichloride;
In
2-ethoxy-ethanol; ethanol; water; acetic acid; acetonitrile;
