thiophosphoramidic acid O,O'-bis-(4-nitro-phenyl) ester

Base Information

Chemical Name:thiophosphoramidic acid O,O'-bis-(4-nitro-phenyl) ester
CAS No.:332095-13-3
Molecular Formula:C₁₂H₁₀N₃O₆PS
Molecular Weight:355.268
Hs Code.:

thiophosphoramidic acid <i>O</i>,<i>O</i>'-bis-(4-nitro-phenyl) ester

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Chemical Property of thiophosphoramidic acid O,O'-bis-(4-nitro-phenyl) ester

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Technology Process of thiophosphoramidic acid O,O'-bis-(4-nitro-phenyl) ester

There total 2 articles about thiophosphoramidic acid O,O'-bis-(4-nitro-phenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52678-80-5
bis(p-nitrophenyl)phosphorochloridothioate

: 332095-13-3
thiophosphoramidic acid O,O'-bis-(4-nitro-phenyl) ester

Guidance literature:: With ammonia; In benzene; at 40 ℃; for 2h;
DOI:10.1080/104265090968064

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 332095-13-3
thiophosphoramidic acid O,O'-bis-(4-nitro-phenyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / thiophosphyl chloride; aq. sodium hydroxide; benzyltriethylammonium chloride / benzene

2: ammonia / benzene / 2 h / 40 °C

With trichlorothiophosphine; sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; ammonia; In benzene;
DOI:10.1080/104265090968064

Reference yield: 58.0%

: 52678-80-5
bis(p-nitrophenyl)phosphorochloridothioate

: 332095-13-3
thiophosphoramidic acid O,O'-bis-(4-nitro-phenyl) ester

: C₂₄H₁₇N₅O₁₂P₂S₂

Guidance literature:: thiophosphoramidic acid O,O'-bis-(4-nitro-phenyl) ester; With sodium hydride; In tetrahydrofuran; for 2h; Heating;

bis(p-nitrophenyl)phosphorochloridothioate; In tetrahydrofuran; for 6h; Heating;
DOI:10.1080/104265090968064