trans-{CoCl₂phn2}Cl

Base Information

Chemical Name:trans-{CoCl₂phn2}Cl
CAS No.:98167-38-5
Molecular Formula:C₁₆H₂₄Cl₂CoN₄*Cl
Molecular Weight:437.746
Hs Code.:

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Chemical Property of trans-{CoCl₂phn2}Cl

Chemical Property:

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Technology Process of trans-{CoCl₂phn2}Cl

There total 3 articles about trans-{CoCl₂phn2}Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: cobalt(II) chloride hexahydrate

: 4921-62-4,16635-94-2,98300-61-9,98300-62-0,132316-54-2
(R/S)-1,2-diamino-1-phenylethane dihydrochloride

: 98167-38-5
trans-{CoCl₂phn2}Cl

Guidance literature:: With sodium hydroxide; air; In water; addn. of d,l-phenylethylenediamine dihydrochloride (0.0625 mol) to aq. soln. of CoCl2*6H2O (0.05 mol); heating to 70°C; addn. of NaOH (pH 8); introduction of air for 24 h;; pptn.; filtering, treating filtrate with concd. HCl and concg.; filtering, washing solid with concd. HCl; dissolving ppt. in abs. ethanol, addn. of concd. HCl; pptn. on concg.; washing with abs. alc. and drying under vac. at 65°C; elem. anal.;;

Reference yield:

: 7647-01-0,15364-23-5
hydrogenchloride

: cobalt(II) chloride hexahydrate

: 5700-56-1
1,2-diaminophenylethane

: 98167-38-5
trans-{CoCl₂phn2}Cl

Guidance literature:: With air; In ethanol; CoCl2*6H2O in alcohol, phenylethylenediamine and concd. HCl-soln.; crystallization on passing of air through the reaction-mixture for 20 h; concn. of the mother-lye;; recrystallization in alc. HCl-soln. and drying at 130°C; contaminated;;