[Re⁽¹⁸⁾O₂(C₅H₅N)4]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Re⁽¹⁸⁾O₂(C₅H₅N)4]B(C₆H₅)4

Base Information

Chemical Name:[Re⁽¹⁸⁾O₂(C₅H₅N)4]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Re⁽¹⁸⁾O₂(C₅H₅N)4]B(C₆H₅)4
CAS No.:84417-13-0
Molecular Formula:C₂₀H₂₀N₄O₂Re*C₂₄H₂₀B
Molecular Weight:857.846
Hs Code.:

[Re<sup>(18)</sup>O<sub>2</sub>(C<sub>5</sub>H<sub>5</sub>N)4]<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup>=[Re<sup>(18)</sup>O<sub>2</sub>(C<sub>5</sub>H<sub>5</sub>N)4]B(C<sub>6</sub>H<sub>5</sub>)4

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Chemical Property of [Re⁽¹⁸⁾O₂(C₅H₅N)4]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Re⁽¹⁸⁾O₂(C₅H₅N)4]B(C₆H₅)4

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Technology Process of [Re⁽¹⁸⁾O₂(C₅H₅N)4]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Re⁽¹⁸⁾O₂(C₅H₅N)4]B(C₆H₅)4

There total 1 articles about [Re⁽¹⁸⁾O₂(C₅H₅N)4]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Re⁽¹⁸⁾O₂(C₅H₅N)4]B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14104-20-2
silver tetrafluoroborate

: potassium hexachlororhenate(IV)

: 143-66-8
sodium tetraphenyl borate

: 14797-71-8
¹⁸O-labeled water

: 84417-13-0
[Re⁽¹⁸⁾O₂(C₅H₅N)4]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Re⁽¹⁸⁾O₂(C₅H₅N)4]B(C₆H₅)4

Guidance literature:: With pyridine; In further solvent(s); K2ReCl6 and AgBF4 were mixed in H2(18)O under Ar, soln. was degassed and dry pyridine was then added, the mixt. was refluxed overnight; solvent was removed, EtOH was added to the residue and the mixt. was filtered, NaBPh4 was added to the filtrate, NaCl was filtered off, petroleum ether was added; IR;