tricarbonyl(2,4-cyclohexadien-1-yldimethylphenylphosphonium)iron tetrafluoroborate

Base Information

Chemical Name:tricarbonyl(2,4-cyclohexadien-1-yldimethylphenylphosphonium)iron tetrafluoroborate
CAS No.:88155-43-5
Molecular Formula:BF₄*C₁₇H₁₈FeO₃P
Molecular Weight:443.953
Hs Code.:

Synonyms:

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Chemical Property of tricarbonyl(2,4-cyclohexadien-1-yldimethylphenylphosphonium)iron tetrafluoroborate

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Technology Process of tricarbonyl(2,4-cyclohexadien-1-yldimethylphenylphosphonium)iron tetrafluoroborate

There total 1 articles about tricarbonyl(2,4-cyclohexadien-1-yldimethylphenylphosphonium)iron tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: tricarbonyl(cyclohexadienyl)iron tetrafluoroborate

: 672-66-2
Dimethyl(phenyl)phosphine

: 83288-03-3,88155-43-5
tricarbonyl(2,4-cyclohexadien-1-yldimethylphenylphosphonium)iron tetrafluoroborate

Guidance literature:: In not given;
DOI:10.1016/S0022-328X(00)81959-2

Reference yield: 90.0%

: 83288-03-3,88155-43-5
tricarbonyl(2,4-cyclohexadien-1-yldimethylphenylphosphonium)iron tetrafluoroborate

: 100-52-7
benzaldehyde

: 83349-62-6,83288-00-0
(1-benzylidenecyclohexa-2,4-diene)tricarbonyliron

Guidance literature:: With sodium hydride; In dichloromethane; Fe-complex dissolved in dry CH2Cl2 under N2, cooled to -78°C, NaH and benzaldehyde (molar ratio 1:2:2) added, warmed slowly to room temp., hydrolysed; product contained two isomers; org. layer sepd., dried (MgSO4), evapd., chromd. (silica gel, pentane);elem. anal.;

Reference yield: 90.0%

: 12170-15-9
[(1,2,3,4,5,6-η)benzaldehyde]tricarbonylchromium

: 83288-03-3,88155-43-5
tricarbonyl(2,4-cyclohexadien-1-yldimethylphenylphosphonium)iron tetrafluoroborate

: tricarbonyl[1-(tricarbonylchromiobenzylidene)cyclohexa-2,4-diene]iron

Guidance literature:: With sodium hydride; In dichloromethane; Fe-complex dissolved in dry CH2Cl2 under N2, cooled to -78°C, NaH and Cr-complex (molar ratio 1:2:2) added, warmed slowly to room temp.,hydrolysed; product contained two isomers; org. layer sepd., dried (MgSO4), evapd., chromd. (thick-layer silica plates, benzene-pentane); elem. anal.;