C₂₄H₂₆Br₃N₃O₃

Base Information

Chemical Name:C₂₄H₂₆Br₃N₃O₃
CAS No.:1452586-97-8
Molecular Formula:C₂₄H₂₆Br₃N₃O₃
Molecular Weight:644.201
Hs Code.:

C<sub>24</sub>H<sub>26</sub>Br<sub>3</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₄H₂₆Br₃N₃O₃

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Technology Process of C₂₄H₂₆Br₃N₃O₃

There total 6 articles about C₂₄H₂₆Br₃N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1452587-24-4
C₂₇H₃₂Br₄N₂O₆

: 124-40-3
dimethyl amine

: 1452586-97-8
C₂₄H₂₆Br₃N₃O₃

Guidance literature:: C₂₇H₃₂Br₄N₂O₆; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 4h;

dimethyl amine; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.bmcl.2013.07.017

Reference yield:

: 1452587-03-9
C₁₂H₁₄Br₃NO₂*BrH

: 1452586-97-8
C₂₄H₂₆Br₃N₃O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h

2.1: hydrogenchloride / 1,4-dioxane / 4 h / 20 °C

2.2: 20 °C

With hydrogenchloride; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.07.017

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 1452586-97-8
C₂₄H₂₆Br₃N₃O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridinium bromochromate / acetic acid / 2 h / 40 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 36 h / 20 °C

3.1: bromine / chloroform / 2 h / 20 °C

4.1: hydrogen bromide; water / methanol / 48 h

5.1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h

6.1: hydrogenchloride / 1,4-dioxane / 4 h / 20 °C

6.2: 20 °C

With hydrogenchloride; pyridinium bromochromate; water; hydrogen bromide; bromine; potassium carbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In 1,4-dioxane; methanol; chloroform; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.07.017