C₁₇H₂₄N₂O₄SSi

Base Information

• Chemical Name: C₁₇H₂₄N₂O₄SSi
• CAS No.: 1413439-83-4
• Molecular Formula: C₁₇H₂₄N₂O₄SSi
• Molecular Weight: 380.54
• Mol file: 1413439-83-4.mol

Synonyms:

Chemical Property of C₁₇H₂₄N₂O₄SSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₄N₂O₄SSi

There total 1 articles about C₁₇H₂₄N₂O₄SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro-trimethyl-silane (75-77-4) + C14H16N2O4S (1413439-96-9) → C17H24N2O4SSi (1413439-83-4)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; at -78 ℃;

DOI:10.1038/nchem.1504

Reference yield:

C17H24N2O4SSi (1413439-83-4) → C17H19N3O2 (1413439-92-5)

Guidance literature:

Multi-step reaction with 4 steps

1: hydrogen; palladium on activated charcoal / ethyl acetate

2: n-butyllithium / diethyl ether / -78 °C

3: cesium fluoride

4: chloro(η⁵-cyclopentadienyl)(1,3-dimesitylimidazol-2-ylidene)nickel(II) / tetrahydrofuran / 40 °C

With n-butyllithium; chloro(η⁵-cyclopentadienyl)(1,3-dimesitylimidazol-2-ylidene)nickel(II); palladium on activated charcoal; hydrogen; cesium fluoride; In tetrahydrofuran; diethyl ether; ethyl acetate;

DOI:10.1038/nchem.1504

Reference yield:

C17H24N2O4SSi (1413439-83-4) → C14H17N3O3S (1413440-01-3) + C14H17N3O3S (1413440-02-4)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogen; palladium on activated charcoal / ethyl acetate

2: n-butyllithium / diethyl ether / -78 °C

3: cesium fluoride

With n-butyllithium; palladium on activated charcoal; hydrogen; cesium fluoride; In diethyl ether; ethyl acetate;

DOI:10.1038/nchem.1504

upstream raw materials:

chloro-trimethyl-silane

C₁₄H₁₆N₂O₄S

Downstream raw materials:

C₁₇H₁₉N₃O₂

C₁₄H₁₇N₃O₃S

C₁₄H₁₇N₃O₃S

C₁₈H₂₃N₃O₄S