C₃₉H₄₅FN₄O₂

Base Information

Chemical Name:C₃₉H₄₅FN₄O₂
CAS No.:1617505-30-2
Molecular Formula:C₃₉H₄₅FN₄O₂
Molecular Weight:620.81
Hs Code.:

C<sub>39</sub>H<sub>45</sub>FN<sub>4</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₉H₄₅FN₄O₂

Chemical Property:

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Technology Process of C₃₉H₄₅FN₄O₂

There total 6 articles about C₃₉H₄₅FN₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1555701-57-9
4-bromo-7-methoxy-3,3-dimethyl-1-(2-nitrophenyl)-2,3-dihydro-1H-indole

: 1617505-30-2
C₃₉H₄₅FN₄O₂

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 50 h / 100 °C / Inert atmosphere; Sealed tube

2: zinc; ammonium chloride / methanol; ethyl acetate / 1 h / 20 °C / Inert atmosphere

3: potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

4: dmap / 0.17 h / 100 °C / Inert atmosphere; Microwave irradiation

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; ammonium chloride; zinc; In methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm5006226

Reference yield:

: 6358-77-6
5-bromo-2-methoxyaniline

: 1617505-30-2
C₃₉H₄₅FN₄O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogenchloride; sodium nitrite / water / -10 °C / Inert atmosphere

2.1: sulfuric acid / ethanol / 2 h / 0 - 20 °C / Inert atmosphere

2.2: 0.75 h / 0 - 20 °C / Inert atmosphere

3.1: 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate / toluene / 16 h / 110 °C / Inert atmosphere; Sealed tube

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 50 h / 100 °C / Inert atmosphere; Sealed tube

5.1: zinc; ammonium chloride / methanol; ethyl acetate / 1 h / 20 °C / Inert atmosphere

6.1: potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

7.1: dmap / 0.17 h / 100 °C / Inert atmosphere; Microwave irradiation

With hydrogenchloride; dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; sodium carbonate; potassium carbonate; ammonium chloride; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; zinc; sodium nitrite; In methanol; ethanol; dichloromethane; water; ethyl acetate; toluene; 2.1: |Fischer Indole Synthesis;
DOI:10.1021/jm5006226

Reference yield:

: 1617505-01-7
2-[4-(4-fluorophenyl)-7-methoxy-3,3-dimethyl-2,3-dihydro-1H-indol-1-yl]aniline

: 1617505-30-2
C₃₉H₄₅FN₄O₂

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

2: dmap / 0.17 h / 100 °C / Inert atmosphere; Microwave irradiation

With dmap; potassium carbonate; In dichloromethane;
DOI:10.1021/jm5006226