(E)-1,10-dibenzyl dec-5-enedioate

Base Information

Chemical Name:(E)-1,10-dibenzyl dec-5-enedioate
CAS No.:1332636-67-5
Molecular Formula:C₂₄H₂₈O₄
Molecular Weight:380.484
Hs Code.:

Synonyms:

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Chemical Property of (E)-1,10-dibenzyl dec-5-enedioate

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Technology Process of (E)-1,10-dibenzyl dec-5-enedioate

There total 3 articles about (E)-1,10-dibenzyl dec-5-enedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 87995-27-5
benzyl hex-5-enoate

: 1332636-67-5
(E)-1,10-dibenzyl dec-5-enedioate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In 1,2-dichloro-ethane; for 2h; Reflux;
DOI:10.1021/jm200553w

Reference yield:

: 87995-27-5
benzyl hex-5-enoate

: 1332636-67-5
(E)-1,10-dibenzyl dec-5-enedioate

: dibenzyl (Z)-dec-5-enedioate

Guidance literature:: With C₃₇H₄₀Cl₂N₂ORuS₂; In tetrahydrofuran; at 22 ℃; for 4h; Overall yield = 14 %; Overall yield = 6.3 mg; stereoselective reaction; Glovebox; Inert atmosphere;
DOI:10.1021/jacs.7b06552

Reference yield:

: 1577-22-6
5-hexenoic acid

: 100-39-0
benzyl bromide

: 1332636-67-5
(E)-1,10-dibenzyl dec-5-enedioate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 14 h / 20 °C

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / 1,2-dichloro-ethane / 2 h / Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; potassium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jm200553w