(2-Azabicyclo[2.2.1]hept-5-en-2-yl)(phenyl)methanone

Base Information

Chemical Name:(2-Azabicyclo[2.2.1]hept-5-en-2-yl)(phenyl)methanone
CAS No.:139927-14-3
Molecular Formula:C13H13NO
Molecular Weight:199.252
Hs Code.:
DSSTox Substance ID:DTXSID60569224
Mol file:139927-14-3.mol

Synonyms:139927-14-3;(2-Azabicyclo[2.2.1]hept-5-en-2-yl)(phenyl)methanone;SCHEMBL10636334;DTXSID60569224

Suppliers and Price of (2-Azabicyclo[2.2.1]hept-5-en-2-yl)(phenyl)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of (2-Azabicyclo[2.2.1]hept-5-en-2-yl)(phenyl)methanone

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:199.099714038
Heavy Atom Count:15
Complexity:291

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2CN(C1C=C2)C(=O)C3=CC=CC=C3

Technology Process of (2-Azabicyclo[2.2.1]hept-5-en-2-yl)(phenyl)methanone

There total 7 articles about (2-Azabicyclo[2.2.1]hept-5-en-2-yl)(phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-88-4
benzoyl chloride

: 6671-85-8,110097-96-6
aza-2 bicyclo<2.2.1>heptene-5

: 139927-14-3
2-benzoyl-2-azabicyclo<2.2.1>hept-5-ene

Guidance literature:: With sodium hydroxide; In diethyl ether; at 20 ℃; for 2h;
DOI:10.3390/11080603

Reference yield:

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 139927-14-3
2-benzoyl-2-azabicyclo<2.2.1>hept-5-ene

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium chloride / methanol; H₂O / 20 °C

2: NaOH / diethyl ether / 2 h / 20 °C

With sodium hydroxide; ammonium chloride; In methanol; diethyl ether; water;
DOI:10.3390/11080603

Reference yield:

: 49805-30-3
2-azabicyclo[2.2.1.]hept-5-en-3-one

: 139927-14-3
(+/-)-2-benzoyl-2-azabicyclo<2.2.1>hept-5-ene

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether; tetrahydrofuran / 7 h / Heating

2: aq. sodium carbonate / diethyl ether; tetrahydrofuran / 14 h / Ambient temperature

With lithium aluminium tetrahydride; sodium carbonate; In tetrahydrofuran; diethyl ether;
DOI:10.1248/cpb.45.255