N->acetyl-L-alanyl 3-methylbutylamide

Base Information

Chemical Name:N->acetyl-L-alanyl 3-methylbutylamide
CAS No.:110582-34-8
Molecular Formula:C₂₃H₃₉N₄O₅P
Molecular Weight:482.56
Hs Code.:

N-<N(phenylmethoxy)carbonyl-<1-amino-3-methylbutyl(amino)phosphinyl>>acetyl-L-alanyl 3-methylbutylamide

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N->acetyl-L-alanyl 3-methylbutylamide

Chemical Property:

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Technology Process of N->acetyl-L-alanyl 3-methylbutylamide

There total 12 articles about N->acetyl-L-alanyl 3-methylbutylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N->acetyl-L-alanyl 3-methylbutylamide

: 110582-34-8,110658-49-6,110658-50-9,110658-51-0
N->acetyl-L-alanyl 3-methylbutylamide

Guidance literature:: With ammonia; In dichloromethane; at 21 ℃; for 0.166667h;

Reference yield:

: 128948-77-6
<(1R)-1-amino>-3-methylbutyl>phosphonic acid

: 110582-34-8,110658-49-6,110658-50-9,110658-51-0
C₂₃H₃₉N₄O₅P

Guidance literature:: Multi-step reaction with 8 steps

1: 95 percent / 9 h / 110 °C

2: 95 percent / 2 N NaOH / methanol / 12 h / 21 °C

3: SOCl₂ / CH₂Cl₂ / 4 h

5: TFA

6: dicyclohexylcarbodiimide

7: 1) isobutylene, trimethylsilyl bromide, 2) MeOH / 1) CH₂Cl₂, r.t.

8: 1) ethyl<(dimethylamino)propyl>carbodiimide, 2) NH₃

With methanol; sodium hydroxide; thionyl chloride; trimethylsilyl bromide; ammonia; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; dicyclohexyl-carbodiimide; trifluoroacetic acid; isobutene; In methanol; dichloromethane;
DOI:10.1021/jo00313a012

Reference yield:

: 128948-78-7
methyl hydrogen ((1R)-1-{N-[(phenylmethoxy)carbonyl]amino}-3-methylbutyl)phosphonate

: 110582-34-8,110658-49-6,110658-50-9,110658-51-0
C₂₃H₃₉N₄O₅P

Guidance literature:: Multi-step reaction with 6 steps

1: SOCl₂ / CH₂Cl₂ / 4 h

3: TFA

4: dicyclohexylcarbodiimide

5: 1) isobutylene, trimethylsilyl bromide, 2) MeOH / 1) CH₂Cl₂, r.t.

6: 1) ethyl<(dimethylamino)propyl>carbodiimide, 2) NH₃

With methanol; thionyl chloride; trimethylsilyl bromide; ammonia; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; dicyclohexyl-carbodiimide; trifluoroacetic acid; isobutene; In dichloromethane;
DOI:10.1021/jo00313a012