methyl hydrogen ((1R)-1-{N-[(phenylmethoxy)carbonyl]amino}-3-methylbutyl)phosphonate

Base Information

Chemical Name:methyl hydrogen ((1R)-1-{N-[(phenylmethoxy)carbonyl]amino}-3-methylbutyl)phosphonate
CAS No.:128948-78-7
Molecular Formula:C₁₄H₂₂NO₅P
Molecular Weight:315.306
Hs Code.:

Synonyms:methyl hydrogen ((1R)-1-{N-[(phenylmethoxy)carbonyl]amino}-3-methylbutyl)phosphonate

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Chemical Property of methyl hydrogen ((1R)-1-{N-[(phenylmethoxy)carbonyl]amino}-3-methylbutyl)phosphonate

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Technology Process of methyl hydrogen ((1R)-1-{N-[(phenylmethoxy)carbonyl]amino}-3-methylbutyl)phosphonate

There total 4 articles about methyl hydrogen ((1R)-1-{N-[(phenylmethoxy)carbonyl]amino}-3-methylbutyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 128948-79-8
(R)-benzyl N-[1-(dimethoxyphosphoryl)-3-methylbutyl]carbamate

: 128948-78-7
methyl hydrogen ((1R)-1-{N-[(phenylmethoxy)carbonyl]amino}-3-methylbutyl)phosphonate

Guidance literature:: With sodium hydroxide; In methanol; at 21 ℃; for 12h;
DOI:10.1021/jo00313a012

Reference yield:

: 128948-77-6
<(1R)-1-amino>-3-methylbutyl>phosphonic acid

: 128948-78-7
methyl hydrogen ((1R)-1-{N-[(phenylmethoxy)carbonyl]amino}-3-methylbutyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 9 h / 110 °C

2: 95 percent / 2 N NaOH / methanol / 12 h / 21 °C

With sodium hydroxide; In methanol;
DOI:10.1021/jo00313a012

Reference yield:

: 88081-77-0
L-Leucine phosphonate

: 128948-78-7
methyl hydrogen ((1R)-1-{N-[(phenylmethoxy)carbonyl]amino}-3-methylbutyl)phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: NaHCO₃, Na₂CO₃, 2 N NaOH / H₂O / Ambient temperature

2: 95 percent / 9 h / 110 °C

3: 95 percent / 2 N NaOH / methanol / 12 h / 21 °C

With sodium hydroxide; sodium hydrogencarbonate; sodium carbonate; In methanol; water;
DOI:10.1021/jo00313a012