syn-(PhPS(C₅H₄)2)2Fe₂

Base Information

Chemical Name:syn-(PhPS(C₅H₄)2)2Fe₂
CAS No.:849114-12-1
Molecular Formula:C₃₂H₂₆Fe₂P₂S₂
Molecular Weight:648.332
Hs Code.:

syn-(PhPS(C<sub>5</sub>H<sub>4</sub>)2)2Fe<sub>2</sub>

Synonyms:

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Chemical Property of syn-(PhPS(C₅H₄)2)2Fe₂

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Technology Process of syn-(PhPS(C₅H₄)2)2Fe₂

There total 4 articles about syn-(PhPS(C₅H₄)2)2Fe₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 1,1'-(ferrocenediyl)phenylphosphine

: 7704-34-9
sulfur

: 849114-12-1,315195-61-0,849115-98-6
[(Fe((C₅H₄)2P(S)C₆H₅))2]

: 849114-12-1,315195-61-0,849115-98-6
syn-(PhPS(C₅H₄)2)2Fe₂

Guidance literature:: In tetrahydrofuran; byproducts: ((C5H4PPh)Fe(C5H4))(n); Irradiation (UV/VIS); under N2, Schlenk techniques; irradn. of soln. of Fe(C5H4)2PPh in THF with mercury arc lamp, sulfur added to suspn., mixt. stirred for 1 d; evapd. under vac., residue dissolved in CH2Cl2, chromy. (silica gel, CH2Cl2), evapd. under vac.; elem. anal.;
DOI:10.1021/om049155w

Reference yield: 9.0%

: 1,1'-(ferrocenediyl)phenylphosphine

: 7704-34-9
sulfur

: 849114-12-1,315195-61-0,849115-98-6
[(Fe((C₅H₄)2P(S)C₆H₅))2]

: 849114-12-1,315195-61-0,849115-98-6
syn-(PhPS(C₅H₄)2)2Fe₂

Guidance literature:: In tetrahydrofuran; byproducts: ((C5H4PPh)Fe(C5H4))(n); Irradiation (UV/VIS); under N2, Schlenk techniques; irradn. of soln. of Fe(C5H4)2PPh in THF with mercury arc lamp, sulfur added to suspn., mixt. stirred for 1 d; evapd. under vac., residue dissolved in CH2Cl2, chromy. (silica gel, CH2Cl2), evapd. under vac.; elem. anal.;
DOI:10.1021/om049155w

Reference yield: 5.3%

: 1,1'-(ferrocenediyl)phenylphosphine

: 75-09-2
dichloromethane

: 7704-34-9
sulfur

: 849114-12-1,315195-61-0,849115-98-6
syn-(PhPS(C₅H₄)2)2Fe₂

: 315195-66-5,849115-97-5,849115-99-7
anti-(PhP(C₅H₄)2)2Fe₂

: 315195-66-5,849115-97-5,849115-99-7
syn-(PhP(C₅H₄)2)2Fe₂

: 1,1'':1'',1'''':1''',1'''''-tris(phenylthiophosphinidene)tris(ferrocene)*2/3dichloromethane

: 1,1'':1',1'''':1''',1'''''-tris(phenylthiophosphinidene)tris(ferrocene)*1/3dichloromethane

Guidance literature:: In diethyl ether; Irradiation (UV/VIS); (N2); irradiation of ethereal soln. of ferrocene deriv. at 0°C for 2.5 h, decantation, evapn., dissolving in CH2Cl2, treatment with sulfur for 3 h; chromy. (Al2O3, THF), evapn., dissolving in CH2Cl2, recycling GPC to obtain three bands, overnight GPC recycling first band, elem. anal.;
DOI:10.1021/om800057w