C₃₃H₅₂ClN₅O₄Si₂

Base Information

Chemical Name:C₃₃H₅₂ClN₅O₄Si₂
CAS No.:1260106-36-2
Molecular Formula:C₃₃H₅₂ClN₅O₄Si₂
Molecular Weight:674.431
Hs Code.:

C<sub>33</sub>H<sub>52</sub>ClN<sub>5</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:

Suppliers and Price of C₃₃H₅₂ClN₅O₄Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₅₂ClN₅O₄Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₅₂ClN₅O₄Si₂

There total 13 articles about C₃₃H₅₂ClN₅O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 1260106-36-2
C₃₃H₅₂ClN₅O₄Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 50 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C

2.2: 18 h / 20 °C

3.1: hydrogen / 5% Pd(II)/C(eggshell) / ethyl acetate / 18 h / Inert atmosphere; Sealed tube

4.1: N-iodo-succinimide / acetonitrile / 18 h / 20 °C

5.1: potassium phosphate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 18 h / 100 °C / Inert atmosphere; Sealed tube

With potassium phosphate; N-iodo-succinimide; hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 5% Pd(II)/C(eggshell); In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; ethyl acetate; acetonitrile; mineral oil;

Reference yield:

: 1489-97-0
ethyl 1,4-dioxaspiro[4.5]decane-8-carboxylate

: 1260106-36-2
C₃₃H₅₂ClN₅O₄Si₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: water; lithium hydroxide monohydrate / tetrahydrofuran; methanol / 20 °C

2.1: tetrahydrofuran / 20 °C / Inert atmosphere; Sealed tube

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere; Sealed tube

4.1: 3 h / 100 °C / Neat (no solvent)

5.1: trichlorophosphate; N,N-dimethyl-aniline / 18 h / 20 °C

5.2: 0 °C

6.1: ammonia / methanol / 18 h / 100 °C / Sealed tube

7.1: hydrogenchloride; water / 1,4-dioxane; ethanol / 80 °C / Sealed tube

8.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 50 °C

9.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C

9.2: 18 h / 20 °C

10.1: hydrogen / 5% Pd(II)/C(eggshell) / ethyl acetate / 18 h / Inert atmosphere; Sealed tube

11.1: N-iodo-succinimide / acetonitrile / 18 h / 20 °C

12.1: potassium phosphate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 18 h / 100 °C / Inert atmosphere; Sealed tube

With hydrogenchloride; potassium phosphate; N-iodo-succinimide; lithium hydroxide monohydrate; ammonia; water; hydrogen; sodium hydride; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane; trichlorophosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 5% Pd(II)/C(eggshell); In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; ethyl acetate; acetonitrile; mineral oil;

Reference yield:

: 17159-79-4
ethyl 4-oxocyclohexane-1-carboxylate

: 1260106-36-2
C₃₃H₅₂ClN₅O₄Si₂

Guidance literature:: Multi-step reaction with 13 steps

1.1: toluene-4-sulfonic acid / benzene / Reflux

2.1: water; lithium hydroxide monohydrate / tetrahydrofuran; methanol / 20 °C

3.1: tetrahydrofuran / 20 °C / Inert atmosphere; Sealed tube

4.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere; Sealed tube

5.1: 3 h / 100 °C / Neat (no solvent)

6.1: trichlorophosphate; N,N-dimethyl-aniline / 18 h / 20 °C

6.2: 0 °C

7.1: ammonia / methanol / 18 h / 100 °C / Sealed tube

8.1: hydrogenchloride; water / 1,4-dioxane; ethanol / 80 °C / Sealed tube

9.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 50 °C

10.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 20 °C

10.2: 18 h / 20 °C

11.1: hydrogen / 5% Pd(II)/C(eggshell) / ethyl acetate / 18 h / Inert atmosphere; Sealed tube

12.1: N-iodo-succinimide / acetonitrile / 18 h / 20 °C

13.1: potassium phosphate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 18 h / 100 °C / Inert atmosphere; Sealed tube

With hydrogenchloride; potassium phosphate; N-iodo-succinimide; lithium hydroxide monohydrate; ammonia; water; hydrogen; sodium hydride; toluene-4-sulfonic acid; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane; trichlorophosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 5% Pd(II)/C(eggshell); In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; ethyl acetate; acetonitrile; mineral oil; benzene;