Technology Process of C21H13(2)HO
There total 6 articles about C21H13(2)HO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate; copper diacetate;
In
decalin;
at 120 ℃;
for 12h;
Inert atmosphere;
DOI:10.1002/anie.201200271
- Guidance literature:
-
Multi-step reaction with 2 steps
1: silver hexafluoroantimonate; acetic acid hydrazide; silver carbonate; tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate / acetic acid / 14 h / 120 °C / Inert atmosphere; Sealed tube
2: silver hexafluoroantimonate; acetic acid hydrazide; silver carbonate; tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate / 14 h / 120 °C / Inert atmosphere; Sealed tube
With
silver hexafluoroantimonate; tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate; acetic acid hydrazide; silver carbonate;
In
acetic acid;
DOI:10.1021/ol4021145
- Guidance literature:
-
Multi-step reaction with 2 steps
1: silver hexafluoroantimonate; acetic acid hydrazide; silver carbonate; tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate / acetic acid / 14 h / 120 °C / Inert atmosphere; Sealed tube
2: silver hexafluoroantimonate; acetic acid hydrazide; silver carbonate; tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate / 14 h / 120 °C / Inert atmosphere; Sealed tube
With
silver hexafluoroantimonate; tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate; acetic acid hydrazide; silver carbonate;
In
acetic acid;
DOI:10.1021/ol4021145
