C₂₅H₃₀N₅O₃⁽¹⁺⁾*Cl^(1-)

Base Information

• Chemical Name: C₂₅H₃₀N₅O₃⁽¹⁺⁾*Cl^(1-)
• CAS No.: 1618136-87-0
• Molecular Formula: C₂₅H₃₀N₅O₃*Cl
• Molecular Weight: 483.998
• Mol file: 1618136-87-0.mol

Synonyms:

Chemical Property of C₂₅H₃₀N₅O₃⁽¹⁺⁾*Cl^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₃₀N₅O₃⁽¹⁺⁾*Cl^(1-)

There total 14 articles about C₂₅H₃₀N₅O₃⁽¹⁺⁾*Cl^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

2-(5-aminopentyl)-9-hydroxy-6-methylellipticinium chloride (1618136-77-8) + N-methyl-N-nitroso-carbamate de p-nitrophenyle (75744-83-1) → C25H30N5O3(1+)*Cl(1-) (1618136-87-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃; for 7h;

DOI:10.1016/j.ejmech.2014.05.032

Reference yield:

1,4,9-trimethyl-9H-carbazole-3-carbaldehyde (18073-18-2) → C25H30N5O3(1+)*Cl(1-) (1618136-87-0)

Guidance literature:

Multi-step reaction with 10 steps

1: benzene / 2 h / Reflux

2: sodium tetrahydroborate / methanol / 2 h / 20 °C

3: pyridine / acetonitrile / 8 h / 20 °C

4: hydrogenchloride / 1,4-dioxane / 3 h / 130 °C

5: hexamethylenetetramine / 0.33 h / Reflux

6: sulfuric acid; dihydrogen peroxide / methanol / 4 h / Reflux

7: N,N-dimethyl-formamide / 12 h / 80 °C

8: Amberlite^? IRA-900 (chloride form) / water / 5 h / 20 °C

9: hydrogenchloride / water / 5 h / 20 °C

10: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 7 h / 0 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; hexamethylenetetramine; sulfuric acid; dihydrogen peroxide; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide; acetonitrile; benzene; 6: |Dakin Phenol Oxidation;

DOI:10.1016/j.ejmech.2014.05.032

Reference yield:

C28H33N3O6S (1618136-61-0) → C25H30N5O3(1+)*Cl(1-) (1618136-87-0)

Guidance literature:

Multi-step reaction with 7 steps

1: hydrogenchloride / 1,4-dioxane / 3 h / 130 °C

2: hexamethylenetetramine / 0.33 h / Reflux

3: sulfuric acid; dihydrogen peroxide / methanol / 4 h / Reflux

4: N,N-dimethyl-formamide / 12 h / 80 °C

5: Amberlite^? IRA-900 (chloride form) / water / 5 h / 20 °C

6: hydrogenchloride / water / 5 h / 20 °C

7: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 7 h / 0 °C

With hydrogenchloride; hexamethylenetetramine; sulfuric acid; dihydrogen peroxide; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide; 3: |Dakin Phenol Oxidation;

DOI:10.1016/j.ejmech.2014.05.032

upstream raw materials:

1,4,9-trimethyl-9H-carbazole-3-carbaldehyde

C₂₈H₃₃N₃O₆S

6-methylellipticine

9-formyl-5,6,11-trimethyl-6H-pyrido<4,3-b>carbazole