Technology Process of 1-(N-(1-(methoxycarbonyl)-ethyl)carboxamido)-3,4-dihydronaphthalene
There total 3 articles about 1-(N-(1-(methoxycarbonyl)-ethyl)carboxamido)-3,4-dihydronaphthalene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; triethylamine; triphenylphosphine;
In
N,N-dimethyl-formamide;
at 50 ℃;
for 24h;
under 750.075 Torr;
chemospecific reaction;
Inert atmosphere;
Reflux;
DOI:10.1016/j.tet.2012.11.033
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine; hydrazine hydrate / methanol / 2.5 h / Reflux
2: iodine; N,N,N',N'-tetramethylguanidine / diethyl ether / 0.5 h / 20 °C / Cooling with ice
3: triethylamine; palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 24 h / 50 °C / 750.08 Torr / Inert atmosphere; Reflux
With
iodine; palladium diacetate; hydrazine hydrate; triethylamine; triphenylphosphine; N,N,N',N'-tetramethylguanidine;
In
methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.11.033
- Guidance literature:
-
Multi-step reaction with 2 steps
1: iodine; N,N,N',N'-tetramethylguanidine / diethyl ether / 0.5 h / 20 °C / Cooling with ice
2: triethylamine; palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 24 h / 50 °C / 750.08 Torr / Inert atmosphere; Reflux
With
iodine; palladium diacetate; triethylamine; triphenylphosphine; N,N,N',N'-tetramethylguanidine;
In
diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.11.033
