10-(4-Bromo-phenyl)-9,9-dimethyl-9,10-dihydro-acridine

Base Information

Chemical Name:10-(4-Bromo-phenyl)-9,9-dimethyl-9,10-dihydro-acridine
CAS No.:1342892-15-2
Molecular Formula:C₂₁H₁₈BrN
Molecular Weight:364.285
Hs Code.:
Mol file:1342892-15-2.mol

Synonyms:

Suppliers and Price of 10-(4-Bromo-phenyl)-9,9-dimethyl-9,10-dihydro-acridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TCI Chemical
10-(4-Bromophenyl)-9,9-dimethyl-9,10-dihydroacridine
1G
$ 230.00

TCI Chemical
10-(4-Bromophenyl)-9,9-dimethyl-9,10-dihydroacridine
200MG
$ 66.00

Crysdot
10-(4-Bromophenyl)-9,9-dimethyl-9,10-dihydroacridine 95+%
1g
$ 300.00

Crysdot
10-(4-Bromophenyl)-9,9-dimethyl-9,10-dihydroacridine 95+%
10g
$ 1490.00

Crysdot
10-(4-Bromophenyl)-9,9-dimethyl-9,10-dihydroacridine 95+%
5g
$ 900.00

Ambeed
10-(4-Bromophenyl)-9,9-dimethyl-9,10-dihydroacridine 98+%
1g
$ 109.00

Ambeed
10-(4-Bromophenyl)-9,9-dimethyl-9,10-dihydroacridine 98+%
10g
$ 642.00

Ambeed
10-(4-Bromophenyl)-9,9-dimethyl-9,10-dihydroacridine 98+%
5g
$ 380.00

AK Scientific
10-(4-Bromophenyl)-9,9-dimethyl-9,10-dihydroacridine
1g
$ 372.00

AK Scientific
10-(4-Bromophenyl)-9,9-dimethyl-9,10-dihydroacridine
200mg
$ 143.00

Total 16 raw suppliers

Chemical Property of 10-(4-Bromo-phenyl)-9,9-dimethyl-9,10-dihydro-acridine

Chemical Property:

Melting Point:173 °C
Boiling Point:451.0±34.0 °C(Predicted)
PKA:-2.97±0.40(Predicted)
Density:1.320±0.06 g/cm3(Predicted)

Purity/Quality:

99%, ^*data from raw suppliers

10-(4-Bromophenyl)-9,9-dimethyl-9,10-dihydroacridine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 10-(4-Bromo-phenyl)-9,9-dimethyl-9,10-dihydro-acridine

There total 3 articles about 10-(4-Bromo-phenyl)-9,9-dimethyl-9,10-dihydro-acridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.76%

: 1342892-15-2
10-(4-bromophenyl)-9,9-dimethyl-9,10-dihydro-acridine

Guidance literature:: With copper(l) iodide; potassium carbonate; In N,N-dimethyl-formamide; at 140 ℃; for 12h;

Reference yield:

: 591-50-4
iodobenzene

: 1342892-15-2
10-(4-bromophenyl)-9,9-dimethyl-9,10-dihydro-acridine

Guidance literature:: Multi-step reaction with 4 steps

1: 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; caesium carbonate; palladium diacetate / toluene / 24 h / Reflux; Inert atmosphere

2: di-isopropyl ether / 6 h / 0 - 50 °C / Inert atmosphere

3: phosphoric acid / 12 h / 20 °C

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; sodium t-butanolate / 5,5-dimethyl-1,3-cyclohexadiene / 24 h / Reflux; Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; phosphoric acid; palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; In 5,5-dimethyl-1,3-cyclohexadiene; di-isopropyl ether; toluene;

Reference yield:

: 134-20-3
2-carbomethoxyaniline

: 1342892-15-2
10-(4-bromophenyl)-9,9-dimethyl-9,10-dihydro-acridine

Guidance literature:: Multi-step reaction with 4 steps

1: 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; caesium carbonate; palladium diacetate / toluene / 24 h / Reflux; Inert atmosphere

2: di-isopropyl ether / 6 h / 0 - 50 °C / Inert atmosphere

3: phosphoric acid / 12 h / 20 °C

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; sodium t-butanolate / 5,5-dimethyl-1,3-cyclohexadiene / 24 h / Reflux; Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; phosphoric acid; palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; In 5,5-dimethyl-1,3-cyclohexadiene; di-isopropyl ether; toluene;