N-<(5-hydroxy-2,11-dimethoxy-3,12,16-trimethyl-1,4,10,13-tetraoxo-5β,6α,9α,14aα,15α-1,5,6,7,9,10,13,14,14a,15-decahydro-6,15-imino-4H-isoquino<3,2-b><3>benzazocin-9-yl)methyl>-2-oxo-propanamide

Base Information

• Chemical Name: N-<(5-hydroxy-2,11-dimethoxy-3,12,16-trimethyl-1,4,10,13-tetraoxo-5β,6α,9α,14aα,15α-1,5,6,7,9,10,13,14,14a,15-decahydro-6,15-imino-4H-isoquino<3,2-b><3>benzazocin-9-yl)methyl>-2-oxo-propanamide
• CAS No.: 132150-87-9
• Molecular Formula: C₂₈H₃₁N₃O₉
• Molecular Weight: 553.569

Synonyms:

Chemical Property of N-<(5-hydroxy-2,11-dimethoxy-3,12,16-trimethyl-1,4,10,13-tetraoxo-5β,6α,9α,14aα,15α-1,5,6,7,9,10,13,14,14a,15-decahydro-6,15-imino-4H-isoquino<3,2-b><3>benzazocin-9-yl)methyl>-2-oxo-propanamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-<(5-hydroxy-2,11-dimethoxy-3,12,16-trimethyl-1,4,10,13-tetraoxo-5β,6α,9α,14aα,15α-1,5,6,7,9,10,13,14,14a,15-decahydro-6,15-imino-4H-isoquino<3,2-b><3>benzazocin-9-yl)methyl>-2-oxo-propanamide

There total 5 articles about N-<(5-hydroxy-2,11-dimethoxy-3,12,16-trimethyl-1,4,10,13-tetraoxo-5β,6α,9α,14aα,15α-1,5,6,7,9,10,13,14,14a,15-decahydro-6,15-imino-4H-isoquino<3,2-b><3>benzazocin-9-yl)methyl>-2-oxo-propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

Isopropyl isocyanate (1795-48-8) → (+/-)-saframycin D (66082-30-2,132203-02-2) + N-<(5-hydroxy-2,11-dimethoxy-3,12,16-trimethyl-1,4,10,13-tetraoxo-5α,6α,9α,14aα,15α-1,5,6,7,9,10,13,14,14a,15-decahydro-6,15-imino-4H-isoquino<3,2-b><3>benzazocin-9-yl)methyl>-2-oxo-propanamide (132150-87-9,132203-03-3) + N-<(5-hydroxy-2,11-dimethoxy-3,12,16-trimethyl-1,4,10,13-tetraoxo-5β,6α,9α,14aα,15α-1,5,6,7,9,10,13,14,14a,15-decahydro-6,15-imino-4H-isoquino<3,2-b><3>benzazocin-9-yl)methyl>-2-oxo-propanamide (132150-87-9,132203-03-3)

Guidance literature:

With selenium(IV) oxide; In 1,4-dioxane; for 72h; Ambient temperature;

DOI:10.1016/S0040-4020(01)90067-5

Reference yield: 40.0%

Isopropyl isocyanate (1795-48-8) → (+/-)-saframycin D (66082-30-2,132203-02-2) + N-<(5-hydroxy-2,11-dimethoxy-3,12,16-trimethyl-1,4,10,13-tetraoxo-5α,6α,9α,14aα,15α-1,5,6,7,9,10,13,14,14a,15-decahydro-6,15-imino-4H-isoquino<3,2-b><3>benzazocin-9-yl)methyl>-2-oxo-propanamide (132150-87-9,132203-03-3) + N-<(5-hydroxy-2,11-dimethoxy-3,12,16-trimethyl-1,4,10,13-tetraoxo-5β,6α,9α,14aα,15α-1,5,6,7,9,10,13,14,14a,15-decahydro-6,15-imino-4H-isoquino<3,2-b><3>benzazocin-9-yl)methyl>-2-oxo-propanamide (132150-87-9,132203-03-3)

Guidance literature:

With selenium(IV) oxide; In 1,4-dioxane; for 72h; Ambient temperature;

DOI:10.1016/S0040-4020(01)90067-5

Reference yield: 19.1%

methanol (67-56-1) + (+/-)-saframycin B (82660-65-9) → (+/-)-saframycin C (66082-29-9,132203-04-4) + N-<(5-hydroxy-2,11-dimethoxy-3,12,16-trimethyl-1,4,10,13-tetraoxo-5β,6α,9α,14aα,15α-1,5,6,7,9,10,13,14,14a,15-decahydro-6,15-imino-4H-isoquino<3,2-b><3>benzazocin-9-yl)methyl>-2-oxo-propanamide (132150-87-9,132203-03-3)

Guidance literature:

With selenium(IV) oxide; for 88h; Ambient temperature;

DOI:10.1016/S0040-4020(01)90067-5

upstream raw materials:

(+/-)-saframycin B

Isopropyl isocyanate

methanol

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