AKOS BBS-00006116

Base Information

• Chemical Name: AKOS BBS-00006116
• CAS No.: 620545-85-9
• Molecular Formula: C₁₃H₈O₄
• Molecular Weight: 228.204
• Mol file: 620545-85-9.mol

Synonyms:

Chemical Property of AKOS BBS-00006116

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

2-(Furan-2-ylmethylene)-6-hydroxybenzofuran-3(2H)-one 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of AKOS BBS-00006116

There total 3 articles about AKOS BBS-00006116 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.5%

furfural (98-01-1) + 2-chloro-1-(2,4-dihydroxyphenyl)ethanone (25015-92-3) → (Z)-2-(2-furanyl)methylene-5-hydroxy-3(2H)-benzofuranone (620545-85-9)

Guidance literature:

With potassium hydroxide; In methanol; water; at 20 ℃;

DOI:10.1002/jhet.2497

Reference yield: 81.6%

furfural (98-01-1) + 6-hydroxybenzofuran-3-one (6272-26-0) → C13H8O4 (620545-85-9)

Guidance literature:

With potassium hydroxide; In water; at 25 ℃;

DOI:10.1002/bkcs.12215

Reference yield:

recorcinol (108-46-3) → (Z)-2-(2-furanyl)methylene-5-hydroxy-3(2H)-benzofuranone (620545-85-9)

Guidance literature:

Multi-step reaction with 2 steps

1: zinc(II) chloride; hydrogenchloride / diethyl ether / 72 h / 0 °C

2: potassium hydroxide / methanol; water / 20 °C

With hydrogenchloride; potassium hydroxide; zinc(II) chloride; In methanol; diethyl ether; water;

DOI:10.1002/jhet.2497

upstream raw materials:

furfural

2-chloro-1-(2,4-dihydroxyphenyl)ethanone

recorcinol

6-hydroxybenzofuran-3-one