dodec-2-enenitrile

Base Information

Chemical Name:dodec-2-enenitrile
CAS No.:97585-03-0
Molecular Formula:C₁₂H₂₁N
Molecular Weight:179.305
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dodec-2-enenitrile

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Technology Process of dodec-2-enenitrile

There total 2 articles about dodec-2-enenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2437-25-4
undecyl cyanide

: 97585-03-0
dodec-2-enenitrile

: 97585-02-9
(E)-dodec-2-enenitrile

Guidance literature:: undecyl cyanide; With n-butyllithium; 2,2,6,6-tetramethylpiperidinyl-lithium; In tetrahydrofuran; hexane; at -40 ℃; for 0.5h; Inert atmosphere;

With zinc(II) chloride; In tetrahydrofuran; hexane; at -40 - 0 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

With bis(η3-allyl-μ-chloropalladium(II)); Allyl acetate; In tetrahydrofuran; at -40 - 60 ℃; for 2h; Overall yield = 93 %; Overall yield = 83.4 mg; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.5b02243