Technology Process of (E)-(R)-14-methylhexadec-8-ene-1-al dimethyl acetal
There total 5 articles about (E)-(R)-14-methylhexadec-8-ene-1-al dimethyl acetal which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran; diethylene glycol dimethyl ether;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 100 percent / HCl / 24 h / Ambient temperature
2: 84 percent / Br2, Ph3P, pyridine / CCl4; CH2Cl2
3: 70 percent / liquid ammonia / 4 h
4: 71 percent / BuLi / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 2 h / -20 °C
5: 78 percent / LAH / tetrahydrofuran; bis-(2-methoxy-ethyl) ether
With
pyridine; hydrogenchloride; lithium aluminium tetrahydride; n-butyllithium; bromine; triphenylphosphine;
In
tetrahydrofuran; tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane; diethylene glycol dimethyl ether; ammonia;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 70 percent / liquid ammonia / 4 h
2: 71 percent / BuLi / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 2 h / -20 °C
3: 78 percent / LAH / tetrahydrofuran; bis-(2-methoxy-ethyl) ether
With
lithium aluminium tetrahydride; n-butyllithium;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; diethylene glycol dimethyl ether; ammonia;