7-bromoheptanal dimethyl acetal

Base Information

Chemical Name:7-bromoheptanal dimethyl acetal
CAS No.:130129-93-0
Molecular Formula:C₉H₁₉BrO₂
Molecular Weight:239.153
Hs Code.:

Synonyms:7-bromoheptanal dimethyl acetal

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Chemical Property of 7-bromoheptanal dimethyl acetal

Chemical Property:

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Technology Process of 7-bromoheptanal dimethyl acetal

There total 1 articles about 7-bromoheptanal dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 67-56-1
methanol

: 54005-84-4
7-bromoheptanal

: 130129-93-0
7-bromoheptanal dimethyl acetal

Guidance literature:: With toluene-4-sulfonic acid; at 20 ℃; for 0.166667h;

Reference yield:

: 130129-93-0
7-bromoheptanal dimethyl acetal

: 130271-88-4,71566-68-2
(Z)-(R)-14-methylhexadec-8-ene-1-al dimethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / liquid ammonia / 4 h

2: 71 percent / BuLi / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 2 h / -20 °C

3: 100 percent / H₂ / Ni

With n-butyllithium; hydrogen; nickel; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; ammonia;

Reference yield:

: 130129-93-0
7-bromoheptanal dimethyl acetal

: 130194-59-1,71566-68-2
(E)-(R)-14-methylhexadec-8-ene-1-al dimethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / liquid ammonia / 4 h

2: 71 percent / BuLi / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide / 2 h / -20 °C

3: 78 percent / LAH / tetrahydrofuran; bis-(2-methoxy-ethyl) ether

With lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; diethylene glycol dimethyl ether; ammonia;