ETHYL 5,6,7,8-TETRAHYDROIMIDAZO[1,2-A]PYRAZINE-2-CARBOXYLATE DIHYDROCHLORIDE 0.5 HYDRATE

Base Information

Chemical Name:ETHYL 5,6,7,8-TETRAHYDROIMIDAZO[1,2-A]PYRAZINE-2-CARBOXYLATE DIHYDROCHLORIDE 0.5 HYDRATE
CAS No.:623564-18-1
Molecular Formula:C₉H₁₃N₃O₂*ClH
Molecular Weight:231.682
Hs Code.:
Mol file:623564-18-1.mol

Synonyms:

Suppliers and Price of ETHYL 5,6,7,8-TETRAHYDROIMIDAZO[1,2-A]PYRAZINE-2-CARBOXYLATE DIHYDROCHLORIDE 0.5 HYDRATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 2 raw suppliers

Chemical Property of ETHYL 5,6,7,8-TETRAHYDROIMIDAZO[1,2-A]PYRAZINE-2-CARBOXYLATE DIHYDROCHLORIDE 0.5 HYDRATE

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ETHYL 5,6,7,8-TETRAHYDROIMIDAZO[1,2-A]PYRAZINE-2-CARBOXYLATE DIHYDROCHLORIDE 0.5 HYDRATE

There total 4 articles about ETHYL 5,6,7,8-TETRAHYDROIMIDAZO[1,2-A]PYRAZINE-2-CARBOXYLATE DIHYDROCHLORIDE 0.5 HYDRATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 77112-52-8
ethyl imidazo[1,2-a]pyrazine-2-carboxylate

: 623564-18-1
5,6,7,8-tetrahydroimidazo[1,2-a]pyrazine-2-carboxylic acid ethyl ester hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 15h; under 2068.59 Torr;
DOI:10.1021/jm060021p

Reference yield:

: HCl-EtOH

: 77112-52-8
ethyl imidazo[1,2-a]pyrazine-2-carboxylate

: 623564-18-1
5,6,7,8-tetrahydroimidazo[1,2-a]pyrazine-2-carboxylic acid ethyl ester hydrochloride

Guidance literature:: Pd-C; In ethanol;

Reference yield:

: 70-23-5
ethyl Bromopyruvate

: 623564-18-1
5,6,7,8-tetrahydroimidazo[1,2-a]pyrazine-2-carboxylic acid ethyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,2-dimethoxy-ethane / 2.5 h / 20 °C

1.2: 22 percent / ethanol / 2 h / Heating

2.1: 63 percent / H₂; HCl / Pd/C / ethanol / 15 h / 20 °C / 2068.59 Torr

With hydrogenchloride; hydrogen; palladium on activated charcoal; In 1,2-dimethoxyethane; ethanol;
DOI:10.1021/jm060021p