(8,9-2H₆)geranyl benzyl ether

Base Information

• Chemical Name: (8,9-2H₆)geranyl benzyl ether
• CAS No.: 149195-06-2
• Molecular Formula: C₁₇H₂₄O
• Molecular Weight: 250.329
• Mol file: 149195-06-2.mol

Synonyms:

Chemical Property of (8,9-2H₆)geranyl benzyl ether

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (8,9-2H₆)geranyl benzyl ether

There total 1 articles about (8,9-2H₆)geranyl benzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-4-methyl-6-(phenylmethoxy)-4-hexenal (32989-52-9) + <1-(2H3)methyl(2-2H3)ethyl>triphenylphosphonium bromide (127208-25-7) → (8,9-2H6)geranyl benzyl ether (149195-06-2)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1.) THF, hexane, rt, 1 h, 2.) rt, 3 h;

DOI:10.1021/jo00067a037

Reference yield: 97.0%

(8,9-2H6)geranyl benzyl ether (149195-06-2) → (8,9-2H6)geraniol (66063-44-3)

Guidance literature:

With ammonia; lithium; In tetrahydrofuran; for 0.5h; Heating;

DOI:10.1021/jo00067a037

upstream raw materials:

(E)-4-methyl-6-(phenylmethoxy)-4-hexenal

<1-(2H3)methyl(2-2H3)ethyl>triphenylphosphonium bromide

Downstream raw materials:

(8,9-2H6)geraniol