APTAB [3-(9-Anthracene)propyl triMethylaMMoniuM broMide]

Base Information

• Chemical Name: APTAB [3-(9-Anthracene)propyl triMethylaMMoniuM broMide]
• CAS No.: 86727-71-1
• Molecular Formula: Br*C₂₀H₂₄N
• Molecular Weight: 358.321
• Mol file: 86727-71-1.mol

Synonyms:

Chemical Property of APTAB [3-(9-Anthracene)propyl triMethylaMMoniuM broMide]

Chemical Property:

Purity/Quality:

>98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of APTAB [3-(9-Anthracene)propyl triMethylaMMoniuM broMide]

There total 3 articles about APTAB [3-(9-Anthracene)propyl triMethylaMMoniuM broMide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ω-(anthracene-9-yl)propanol (22689-05-0) → <3-(9-anthracenyl)propyl>trimethylammonium bromide (86727-71-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / 48percent HBr, red phosphorus / 40 h / Heating

2: ethanol / 4 h / Heating

With phosphorus; hydrogen bromide; In ethanol;

DOI:10.1021/j100245a020

Reference yield:

3-anthracen-9-ylpropionic acid (41034-83-7) → <3-(9-anthracenyl)propyl>trimethylammonium bromide (86727-71-1)

Guidance literature:

Multi-step reaction with 3 steps

1: LiAlH₄ / tetrahydrofuran

2: 85 percent / 48percent HBr, red phosphorus / 40 h / Heating

3: ethanol / 4 h / Heating

With phosphorus; lithium aluminium tetrahydride; hydrogen bromide; In tetrahydrofuran; ethanol;

DOI:10.1021/j100245a020

Reference yield:

3-(9-anthracenyl)propyl bromide (22756-32-7) + trimethylamine (75-50-3) → <3-(9-anthracenyl)propyl>trimethylammonium bromide (86727-71-1)

Guidance literature:

In ethanol; for 4h; Heating;

DOI:10.1021/j100245a020

upstream raw materials:

3-(9-anthracenyl)propyl bromide

trimethylamine

ω-(anthracene-9-yl)propanol

3-anthracen-9-ylpropionic acid

Refernces