deacetyl-O-methylshikoccin

Base Information

• Chemical Name: deacetyl-O-methylshikoccin
• CAS No.: 96737-07-4
• Molecular Formula: C₂₁H₃₀O₄
• Molecular Weight: 346.467

Synonyms:

Chemical Property of deacetyl-O-methylshikoccin

Chemical Property:

Purity/Quality:

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Technology Process of deacetyl-O-methylshikoccin

There total 1 articles about deacetyl-O-methylshikoccin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + shikoccin (73211-11-7) → O-methylshikoccin (83159-26-6,122741-65-5) + deacetyl-O-methylshikoccin (96737-07-4) + Acetic acid (2R,4R,6S,9R,13R)-2-methoxy-14-methoxymethyl-5,5,9-trimethyl-10,15-dioxo-tricyclo[11.2.1.04,9]hexadec-1(16)-en-6-yl ester

Guidance literature:

With sulfuric acid; for 45h; Heating;

Reference yield: 88.0%

acetic anhydride (108-24-7) + deacetyl-O-methylshikoccin (96737-07-4) → O-methylshikoccin (83159-26-6,122741-65-5)

Guidance literature:

With pyridine; dmap; In dichloromethane;

DOI:10.1021/ja971527n

upstream raw materials:

methanol

shikoccin

Downstream raw materials:

O-methylshikoccin

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