methyl 5-<2-formyl-3-(6-hydroxy-5-hydroxymethyl-3-methylocta-1,3-dienyl)-4-methylcyclopent-2-enyl>-5-<α-L-mycarosyl-(1->4)-β-D-mycaminosyloxy>valerate

Base Information

• Chemical Name: methyl 5-<2-formyl-3-(6-hydroxy-5-hydroxymethyl-3-methylocta-1,3-dienyl)-4-methylcyclopent-2-enyl>-5-<α-L-mycarosyl-(1->4)-β-D-mycaminosyloxy>valerate
• CAS No.: 121512-85-4
• Molecular Formula: C₃₉H₆₅NO₁₃
• Molecular Weight: 755.944
• Mol file: 121512-85-4.mol

Synonyms:

Chemical Property of methyl 5-<2-formyl-3-(6-hydroxy-5-hydroxymethyl-3-methylocta-1,3-dienyl)-4-methylcyclopent-2-enyl>-5-<α-L-mycarosyl-(1->4)-β-D-mycaminosyloxy>valerate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 5-<2-formyl-3-(6-hydroxy-5-hydroxymethyl-3-methylocta-1,3-dienyl)-4-methylcyclopent-2-enyl>-5-<α-L-mycarosyl-(1->4)-β-D-mycaminosyloxy>valerate

There total 1 articles about methyl 5-<2-formyl-3-(6-hydroxy-5-hydroxymethyl-3-methylocta-1,3-dienyl)-4-methylcyclopent-2-enyl>-5-<α-L-mycarosyl-(1->4)-β-D-mycaminosyloxy>valerate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2',4'',20-tri-O-acetyl-2''',3'''-didehydro-2'''-demethoxy-4'''-deoxy-4'''-oxotylosin 3,20-hemiacetal (121530-10-7) → methyl 5-<2-formyl-3-(6-hydroxy-5-hydroxymethyl-3-methylocta-1,3-dienyl)-4-methylcyclopent-2-enyl>-5-<α-L-mycarosyl-(1->4)-β-D-mycaminosyloxy>valerate (121512-85-4) + 23-demycinosyltylosin (79592-92-0)

Guidance literature:

With sodium methylate; triethylamine; Yield given. Multistep reaction. Yields of byproduct given; 1.) methanol, 25 deg C, 1 h, 2.) 40 deg C, 67 h;

DOI:10.1039/P19890000775

upstream raw materials:

2',4'',20-tri-O-acetyl-2''',3'''-didehydro-2'''-demethoxy-4'''-deoxy-4'''-oxotylosin 3,20-hemiacetal