1-methyl-1-octylpyrrolidinium chloride

Base Information

• Chemical Name: 1-methyl-1-octylpyrrolidinium chloride
• CAS No.: 909398-60-3
• Molecular Formula: C₁₃H₂₈N*Cl
• Molecular Weight: 233.825
• Mol file: 909398-60-3.mol

Synonyms:

Chemical Property of 1-methyl-1-octylpyrrolidinium chloride

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-methyl-1-octylpyrrolidinium chloride

There total 4 articles about 1-methyl-1-octylpyrrolidinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-Methylpyrrolidine (120-94-5) + n-chlorooctane (111-85-3) → 1-methyl-1-octylpyrrolidinium chloride (909398-60-3)

Guidance literature:

at 120 - 180 ℃; for 1.08333h; microwave irradiation;

DOI:10.3390/molecules13010149

Reference yield: 93.0%

1-methyl-1-octylpyrrolidin-1-ium bromide (1133731-86-8) → 1-methyl-1-octylpyrrolidinium chloride (909398-60-3)

Guidance literature:

With Amberlite-IRA₄₀₀ (Cl) ion-exchange resin; In methanol;

DOI:10.1039/c4cc05505e

Reference yield:

1-Methylpyrrolidine (120-94-5) → 1-methyl-1-octylpyrrolidinium chloride (909398-60-3)

Guidance literature:

Multi-step reaction with 2 steps

1: ethyl acetate / 24 h / 40 °C

2: Amberlite-IRA₄₀₀ (Cl) ion-exchange resin / methanol

With Amberlite-IRA₄₀₀ (Cl) ion-exchange resin; In methanol; ethyl acetate;

DOI:10.1039/c4cc05505e

upstream raw materials:

1-Methylpyrrolidine

n-chlorooctane

1-bromo-octane

1-methyl-1-octylpyrrolidin-1-ium bromide

Downstream raw materials:

1-octyl-3-methylpyrrolidinium bis((trifluoromethyl)sulfonyl)imide