N-methoxy-N-methyl-5,6-dihydro-4H-pyrrolo[1,2-b]pyrazole-2-carboxamide

Base Information

Chemical Name:N-methoxy-N-methyl-5,6-dihydro-4H-pyrrolo[1,2-b]pyrazole-2-carboxamide
CAS No.:799781-97-8
Molecular Formula:C₉H₁₃N₃O₂
Molecular Weight:195.221
Hs Code.:
DSSTox Substance ID:DTXSID20463330
Wikidata:Q82288186
Mol file:799781-97-8.mol

Synonyms:N-methoxy-N-methyl-5,6-dihydro-4H-pyrrolo[1,2-b]pyrazole-2-carboxamide;799781-97-8;SCHEMBL4821143;DTXSID20463330;FWHHOSCDELSADD-UHFFFAOYSA-N;AG-H-20459;N-methoxy-N-methyl-5,6-dihydro-4H-pyrrolo-[1,2-b]pyrazole-2-carboxamide;N-methoxy-N-methyl-5,6-dihydro-4H-pyrrolo[1,2-b]-pyrazole-2-carboxamide

Suppliers and Price of N-methoxy-N-methyl-5,6-dihydro-4H-pyrrolo[1,2-b]pyrazole-2-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N-METHOXY-N-METHYL-5,6-DIHYDRO-4H-PYRROLO[1,2-B]PYRAZOLE-2-CARBOXAMIDE 95.00%
5MG
$ 504.12

Alichem
N-Methoxy-N-methyl-5,6-dihydro-4H-pyrrolo[1,2-b]pyrazole-2-carboxamide
10g
$ 1969.80

Alichem
N-Methoxy-N-methyl-5,6-dihydro-4H-pyrrolo[1,2-b]pyrazole-2-carboxamide
5g
$ 1460.60

Total 3 raw suppliers

Chemical Property of N-methoxy-N-methyl-5,6-dihydro-4H-pyrrolo[1,2-b]pyrazole-2-carboxamide

Chemical Property:

XLogP3:0.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:195.100776666
Heavy Atom Count:14
Complexity:234

Purity/Quality:

97% ^*data from raw suppliers

N-METHOXY-N-METHYL-5,6-DIHYDRO-4H-PYRROLO[1,2-B]PYRAZOLE-2-CARBOXAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C(=O)C1=NN2CCCC2=C1)OC

Technology Process of N-methoxy-N-methyl-5,6-dihydro-4H-pyrrolo[1,2-b]pyrazole-2-carboxamide

There total 2 articles about N-methoxy-N-methyl-5,6-dihydro-4H-pyrrolo[1,2-b]pyrazole-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: C₇H₇ClN₂O

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 799781-97-8
N-methoxy-N-methyl-5,6-dihydro-4H-pyrrolo-[1,2-b]pyrazole-2-carboxamide

Guidance literature:: With potassium carbonate; In dichloromethane; water; at 10 - 20 ℃; for 1.65 - 2h;

Reference yield:

: potassium 5,6-dihydro-4H-pyrrolo-[1,2-b]pyrazole-2-carboxylate

: 799781-97-8
N-methoxy-N-methyl-5,6-dihydro-4H-pyrrolo-[1,2-b]pyrazole-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / dichloromethane; N,N-dimethyl-formamide / 1.75 h / 28 °C / Inert atmosphere; Large scale

2: potassium carbonate / water / 1.75 h / 10 - 20 °C / Large scale

With thionyl chloride; potassium carbonate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/op050218b