(4Z,7Z,10Z,13Z,16Z,19Z)-docosa-4,7,10,13,16,19-hexaenoic acid trans-2-phenyl-[1,3]dioxan-5-yl ester

Base Information

• Chemical Name: (4Z,7Z,10Z,13Z,16Z,19Z)-docosa-4,7,10,13,16,19-hexaenoic acid trans-2-phenyl-[1,3]dioxan-5-yl ester
• CAS No.: 1258497-47-0
• Molecular Formula: C₃₂H₄₂O₄
• Molecular Weight: 490.683
• Mol file: 1258497-47-0.mol

Synonyms:

Chemical Property of (4Z,7Z,10Z,13Z,16Z,19Z)-docosa-4,7,10,13,16,19-hexaenoic acid trans-2-phenyl-[1,3]dioxan-5-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4Z,7Z,10Z,13Z,16Z,19Z)-docosa-4,7,10,13,16,19-hexaenoic acid trans-2-phenyl-[1,3]dioxan-5-yl ester

There total 1 articles about (4Z,7Z,10Z,13Z,16Z,19Z)-docosa-4,7,10,13,16,19-hexaenoic acid trans-2-phenyl-[1,3]dioxan-5-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

docosahexaenoic acid (6217-54-5) + benzaldehyde (100-52-7) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → (4Z,7Z,10Z,13Z,16Z,19Z)-docosa-4,7,10,13,16,19-hexaenoic acid trans-(2-phenyl-[1,3]dioxolan-4-yl)methyl ester + (4Z,7Z,10Z,13Z,16Z,19Z)-docosa-4,7,10,13,16,19-hexaenoic acid cis-(2-phenyl-[1,3]dioxolan-4-yl)methyl ester + (4Z,7Z,10Z,13Z,16Z,19Z)-docosa-4,7,10,13,16,19-hexaenoic acid trans-2-phenyl-[1,3]dioxan-5-yl ester (1258497-47-0) + (4Z,7Z,10Z,13Z,16Z,19Z)-docosa-4,7,10,13,16,19-hexaenoic acid cis-2-phenyl-[1,3]dioxan-5-yl ester (1258497-46-9)

Guidance literature:

benzaldehyde; glycerol; Inert atmosphere;

docosahexaenoic acid; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 96h; Inert atmosphere;

DOI:10.1016/j.tet.2010.09.070

upstream raw materials:

docosahexaenoic acid

benzaldehyde

glycerol