tert-butyl 15-bromopentadecanoate

Base Information

Chemical Name:tert-butyl 15-bromopentadecanoate
CAS No.:905302-64-9
Molecular Formula:C₁₉H₃₇BrO₂
Molecular Weight:377.406
Hs Code.:

Synonyms:

Suppliers and Price of tert-butyl 15-bromopentadecanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of tert-butyl 15-bromopentadecanoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl 15-bromopentadecanoate

There total 6 articles about tert-butyl 15-bromopentadecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 56523-59-2
15-bromo-pentadecanoic acid

: 75-65-0
tert-butyl alcohol

: 905302-64-9
tert-butyl 15-bromopentadecanoate

Guidance literature:: 15-bromo-pentadecanoic acid; With trifluoroacetic anhydride; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere; Darkness;

tert-butyl alcohol; In dichloromethane; for 3h; Inert atmosphere; Darkness;
DOI:10.1039/c6cc09305a

Reference yield: 75.0%

: 905302-64-9
tert-butyl 15-bromopentadecanoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 0.5h; Cooling with ice;

In dichloromethane; at 20 ℃;

Reference yield:

: 4617-33-8
15-hydroxylpentadecanoic acid

: 905302-64-9
tert-butyl 15-bromopentadecanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen bromide; acetic acid; sulfuric acid / water / 4 h / 110 °C / Inert atmosphere

2.1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

With thionyl chloride; sulfuric acid; hydrogen bromide; acetic acid; N,N-dimethyl-formamide; In dichloromethane; water;
DOI:10.1039/c9cc09993j