tert-butyl-bis(trimethylsilyl)stibine

Base Information

Chemical Name:tert-butyl-bis(trimethylsilyl)stibine
CAS No.:82363-93-7
Molecular Formula:C₁₀H₂₇SbSi₂
Molecular Weight:325.245
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl-bis(trimethylsilyl)stibine

Chemical Property:

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Technology Process of tert-butyl-bis(trimethylsilyl)stibine

There total 2 articles about tert-butyl-bis(trimethylsilyl)stibine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 75-77-4
chloro-trimethyl-silane

: 4718-00-7
di-tert-butylantimony chloride

: 13787-35-4
Tri-tert-butyl-stibane

: 82363-94-8
t-Bu₂SbSiMe₃

: 82363-93-7
tert-butyl-bis(trimethylsilyl)stibine

: 4791-75-7
{(t-C₄H₉)2Sb}2

: 4791-73-5
tetra-tert.-butylcyclotetrastibane

Guidance literature:: With magnesium; In tetrahydrofuran; byproducts: MgCl2; (Ar), soln. of the Sb-compd. droped under stirring within 2 h to Me3SiCl and Mg-chips, stirred for further 10 h at room temp.; solvent evapd. at 0.01 mm Hg, washed 5 times with pentane, solvent removed at reduced pressure, NMR, distilled at 68°C/0.01 mm Hg, elem.anal.;

Reference yield: 40.0%

: 75-77-4
chloro-trimethyl-silane

: 67877-43-4
t-BuSbCl₂

: 13787-35-4
Tri-tert-butyl-stibane

: 82363-94-8
t-Bu₂SbSiMe₃

: 82363-93-7
tert-butyl-bis(trimethylsilyl)stibine

: 7029-27-8
tris(trimethylsilyl)antimony

Guidance literature:: With magnesium; In tetrahydrofuran; byproducts: MgCl2; (Ar), Sb-compd. in THF droped to Me3SiCl and Mg-chips in THF, stirred for 10 h; solvent evapd. at 0.01 mm Hg, washed 5 times with pentane, solvent removed at reduced pressure, NMR, distilled;