(2,6-bis[(di-t-butylphosphino)methyl]phenyl)hydridonickel

Base Information

• Chemical Name: (2,6-bis[(di-t-butylphosphino)methyl]phenyl)hydridonickel
• CAS No.: 60399-53-3
• Molecular Formula: C₂₄H₄₄NiP₂
• Molecular Weight: 453.251
• Mol file: 60399-53-3.mol

Synonyms:

Chemical Property of (2,6-bis[(di-t-butylphosphino)methyl]phenyl)hydridonickel

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (2,6-bis[(di-t-butylphosphino)methyl]phenyl)hydridonickel

There total 1 articles about (2,6-bis[(di-t-butylphosphino)methyl]phenyl)hydridonickel which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[CpW(CO)2(μ-κ,C:κ,O-CO)Ni(tBuPCP)] (1277178-87-6) + hydrogen (1333-74-0) → tricarbonylcyclopentadienyltungsten(II) hydride (12128-26-6) + (2,6-bis[(di-t-butylphosphino)methyl]phenyl)hydridonickel (60399-53-3)

Guidance literature:

In nitromethane-d3; pressurized with H2 at 30 bar for 18 h at room temp., heated at 60°C for 2 h;

DOI:10.1002/anie.201005274

upstream raw materials:

[CpW(CO)₂(μ-κ,C:κ,O-CO)Ni(^tBuPCP)]

hydrogen