ethyl trans-3-hydroxy-1-methylcyclobutanecarboxylate

Base Information

Chemical Name:ethyl trans-3-hydroxy-1-methylcyclobutanecarboxylate
CAS No.:1408074-59-8
Molecular Formula:C₈H₁₄O₃
Molecular Weight:158.197
Hs Code.:

Synonyms:

Suppliers and Price of ethyl trans-3-hydroxy-1-methylcyclobutanecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Synthonix
Ethyltrans-3-hydroxy-1-methylcyclobutanecarboxylate 95+%
1g
$ 1320.00

Matrix Scientific
Ethyltrans-3-hydroxy-1-methyl-cyclobutanecarboxylate 95+%
1g
$ 2327.00

Crysdot
Ethyltrans-3-hydroxy-1-methyl-cyclobutanecarboxylate 95+%
1g
$ 1382.00

Total 4 raw suppliers

Chemical Property of ethyl trans-3-hydroxy-1-methylcyclobutanecarboxylate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Ethyltrans-3-hydroxy-1-methylcyclobutanecarboxylate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl trans-3-hydroxy-1-methylcyclobutanecarboxylate

There total 4 articles about ethyl trans-3-hydroxy-1-methylcyclobutanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 227607-44-5
ethyl 1-methyl-3-oxocyclobutane-1-carboxylate

: 1408074-59-8
ethyl trans-3-hydroxy-1-methylcyclobutanecarboxylate

Guidance literature:: With ketoreductase MIF₂₀; NADP; In isopropyl alcohol; pH=7; Aqueous phosphate buffer; Enzymatic reaction;

Reference yield:

: 87121-89-9
ethyl 3-oxocyclobutanecarboxylate

: 1408074-59-8
ethyl trans-3-hydroxy-1-methylcyclobutanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / toluene / Reflux

2.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

2.2: -78 - 20 °C

3.1: hydrogenchloride / water; acetone / 96 h / 20 °C

3.2: 2 h / 20 °C

3.3: 1 h

4.1: NADP; ketoreductase MIF₂₀ / isopropyl alcohol / pH 7 / Aqueous phosphate buffer; Enzymatic reaction

With hydrogenchloride; n-butyllithium; sulfuric acid; ketoreductase MIF₂₀; NADP; diisopropylamine; In tetrahydrofuran; water; isopropyl alcohol; acetone; toluene;

Reference yield:

: 1415574-16-1
ethyl 5,8-dioxaspiro[3.4]octane-2-carboxylate

: 1408074-59-8
ethyl trans-3-hydroxy-1-methylcyclobutanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

1.2: -78 - 20 °C

2.1: hydrogenchloride / water; acetone / 96 h / 20 °C

2.2: 2 h / 20 °C

2.3: 1 h

3.1: NADP; ketoreductase MIF₂₀ / isopropyl alcohol / pH 7 / Aqueous phosphate buffer; Enzymatic reaction

With hydrogenchloride; n-butyllithium; ketoreductase MIF₂₀; NADP; diisopropylamine; In tetrahydrofuran; water; isopropyl alcohol; acetone;