(E)-dec-5-enedioic dimethyl ester

Base Information

• Chemical Name: (E)-dec-5-enedioic dimethyl ester
• CAS No.: 4528-48-7
• Molecular Formula: C₁₂H₂₀O₄
• Molecular Weight: 228.288
• Mol file: 4528-48-7.mol

Synonyms:

Chemical Property of (E)-dec-5-enedioic dimethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-dec-5-enedioic dimethyl ester

There total 2 articles about (E)-dec-5-enedioic dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + (Z)-(R)-N,N'-(dec-5-ene-1,10-dioyl)-1,1'-binaphthyl-2,2'-diamine → (Z)-dec-5-enedioic dimethyl ester (4528-48-7) + (R)-1,1'-binaphthyl-2,2'-diamine (18741-85-0)

Guidance literature:

With sulfuric acid; Heating;

DOI:10.1039/b111122c

Reference yield:

methanol (67-56-1) + (E)-(R)-N,N'-(dec-5-ene-1,10-dioyl)-1,1'-binaphthyl-2,2'-diamine → (E)-dec-5-enedioic dimethyl ester (4528-48-7) + (R)-1,1'-binaphthyl-2,2'-diamine (18741-85-0)

Guidance literature:

With sulfuric acid; Heating;

DOI:10.1039/b111122c

Reference yield:

(E)-dec-5-enedioic dimethyl ester (4528-48-7) → 2-hydroxycyclodecanone (96-00-4)

Guidance literature:

Multi-step reaction with 2 steps

1: Na / xylene

2: H₂ / Pt

With hydrogen; sodium; platinum; In xylene;

DOI:10.1021/ja01509a047

upstream raw materials:

methanol

Downstream raw materials:

2-hydroxycyclodecanone