Ethyl 2-cyano-2-(2-nitrophenyl)acetate

Base Information

Chemical Name:Ethyl 2-cyano-2-(2-nitrophenyl)acetate
CAS No.:65548-02-9
Molecular Formula:C11H10 N2 O4
Molecular Weight:234.211
Hs Code.:2926909090
DSSTox Substance ID:DTXSID80372919
Nikkaji Number:J514.438H
Mol file:65548-02-9.mol

Synonyms:ethyl 2-cyano-2-(2-nitrophenyl)acetate;65548-02-9;ethyl cyano(2-nitrophenyl)acetate;Oprea1_863639;SCHEMBL7677183;ethyl cyano-2-nitrophenylacetate;ethyl cyano(o-nitrophenyl)acetate;DTXSID80372919;JUGQARWTQZEZRI-UHFFFAOYSA-N;MFCD01443741;STL134858;AKOS004907489;ethyl (+/-)-cyano(2-nitrophenyl)acetate;CS-0213426;FT-0668211;4K-921;W15325;2-Nitro-alpha-cyanobenzeneacetic acid ethyl ester;F6782-3797

Suppliers and Price of Ethyl 2-cyano-2-(2-nitrophenyl)acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
EthylCyano(2-nitrophenyl)acetate
2g
$ 235.00

Medical Isotopes, Inc.
EthylCyano(2-nitrophenyl)acetate
5 g
$ 1760.00

Crysdot
Ethyl2-cyano-2-(2-nitrophenyl)acetate 97%
25g
$ 1665.00

Crysdot
Ethyl2-cyano-2-(2-nitrophenyl)acetate 97%
5g
$ 550.00

Crysdot
Ethyl2-cyano-2-(2-nitrophenyl)acetate 97%
1g
$ 212.00

American Custom Chemicals Corporation
ETHYL 2-CYANO-2-(2-NITROPHENYL)ACETATE 95.00%
1G
$ 716.10

American Custom Chemicals Corporation
ETHYL 2-CYANO-2-(2-NITROPHENYL)ACETATE 95.00%
10G
$ 2148.30

Alichem
Ethyl2-cyano-2-(2-nitrophenyl)acetate
10g
$ 901.60

Alichem
Ethyl2-cyano-2-(2-nitrophenyl)acetate
5g
$ 550.00

Total 7 raw suppliers

Chemical Property of Ethyl 2-cyano-2-(2-nitrophenyl)acetate

Chemical Property:

Vapor Pressure:1.13E-06mmHg at 25°C
Melting Point:49-51oC
Boiling Point:402°C at 760 mmHg
Flash Point:196.9°C
PSA：95.91000
Density:1.292g/cm³
LogP:2.28828
Storage Temp.:Refrigerator
Solubility.:Chloroform, Methanol
XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:234.06405680
Heavy Atom Count:17
Complexity:341

Purity/Quality:

98% ^*data from raw suppliers

EthylCyano(2-nitrophenyl)acetate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(C#N)C1=CC=CC=C1[N+](=O)[O-]
Uses Ethyl Cyano(2-nitrophenyl)acetate (cas# 65548-02-9) is a compound useful in organic synthesis.

Technology Process of Ethyl 2-cyano-2-(2-nitrophenyl)acetate

There total 7 articles about Ethyl 2-cyano-2-(2-nitrophenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 105-56-6
ethyl 2-cyanoacetate

: 1493-27-2,127723-77-7
ortho-nitrofluorobenzene

: 65548-02-9
(+/-)-ethyl cyano(2-nitrophenyl)acetate

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; 1.) 10 min, 2.) 90 deg C, 0.5 h;
DOI:10.1021/jo00101a046

Reference yield: 99.0%

: 105-56-6
ethyl 2-cyanoacetate

: 528-29-0
1,2-Dinitrobenzene

: 65548-02-9
(+/-)-ethyl cyano(2-nitrophenyl)acetate

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; 1.) 10 min, 2.) 90 deg C, 0.5 h;
DOI:10.1021/jo00101a046

Reference yield: 90.9%

: 88-73-3
2-Chloronitrobenzene

: sodium salt of ethyl cyanoacetate

: 65548-02-9
(+/-)-ethyl cyano(2-nitrophenyl)acetate

Guidance literature:: In dimethyl sulfoxide; at 90 ℃; for 4h; Product distribution; Mechanism; or reaction of o-nitrobromobenzene; addition of small amounts of electron acceptors (o-, m-, p-dinitrobenzene) or radical scavengers (as galvinoxyl, 2-methyl-2-nitrosopropane dimer, phenyl tert-butyl nitrone, hydroquinone, etc.);
DOI:10.1021/jo00053a040