tetraethylammonium tetraiodoferrate(III)

Base Information

• Chemical Name: tetraethylammonium tetraiodoferrate(III)
• CAS No.: 25478-69-7
• Molecular Formula: C₈H₂₀N*FeI₄
• Molecular Weight: 693.719
• Mol file: 25478-69-7.mol

Synonyms:

Chemical Property of tetraethylammonium tetraiodoferrate(III)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetraethylammonium tetraiodoferrate(III)

There total 7 articles about tetraethylammonium tetraiodoferrate(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetraethylammonium iodide (68-05-3) + iodine (7553-56-2,12190-71-5,8031-47-8) + iron (7439-89-6) → tetraethylammonium tetraiodoferrate(III) (25478-69-7)

Guidance literature:

In nitromethane; molar ratio Fe:I2:NR4I 2:3:2, stirring (2 h, 70°C); concn.;

DOI:10.1002/zaac.19966220508

Reference yield:

tetraethylammonium iodide (68-05-3) + iodine (7553-56-2,12190-71-5,8031-47-8) + iron (7439-89-6) + sulfur (7704-34-9) → tetraethylammonium tetraiodoferrate(III) (25478-69-7) + 2N(C2H5)4(1+)*Fe6S6I6(2-)=[N(C2H5)4]2[Fe6S6I6]

Guidance literature:

In tetrahydrofuran; N2-atmosphere; stoich. amts., refluxing for 48 h; evapn., CH2Cl2 addn., standing at 253 K for 3 d; product mixt. not sepd., detd. by IR and Moessbauer spectroscopy;

DOI:10.1016/S0020-1693(98)00301-6

Reference yield:

tetraethylammonium iodide (68-05-3) + iodine (7553-56-2,12190-71-5,8031-47-8) + iron (7439-89-6) + sulfur (7704-34-9) → tetraethylammonium tetraiodoferrate(III) (25478-69-7) + 2N(C2H5)4(1+)*Fe2S2I4(2-)=[N(C2H5)4]2[Fe2S2I4]

Guidance literature:

In tetrahydrofuran; N2-atmosphere; stoich. amts., refluxing for 48 h; concn., CH2Cl2 addn., stirring for 2 h, then standing at 253 K for several d; product mixt. not sepd., detd. by IR and Moessbauer spectroscopy;

DOI:10.1016/S0020-1693(98)00301-6

upstream raw materials:

tetraethylammonium iodide

iodine

iron

sulfur