Technology Process of (2-Ethylpyrrolidin-2-yl)methanol
There total 4 articles about (2-Ethylpyrrolidin-2-yl)methanol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
methanol;
at 50 ℃;
under 760.051 Torr;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride / ethyl acetate / 4 h / 20 °C
1.2: Reflux
2.1: lithium diisopropyl amide / tetrahydrofuran / 3 h / -50 - -20 °C
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
4.1: palladium 10% on activated carbon; hydrogen / methanol / 50 °C / 760.05 Torr
With
hydrogenchloride; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium diisopropyl amide / tetrahydrofuran / 3 h / -50 - -20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
3: palladium 10% on activated carbon; hydrogen / methanol / 50 °C / 760.05 Torr
With
lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; lithium diisopropyl amide;
In
tetrahydrofuran; methanol;