C₂₇H₃₇O₃PS

Base Information

• Chemical Name: C₂₇H₃₇O₃PS
• CAS No.: 1609652-86-9
• Molecular Formula: C₂₇H₃₇O₃PS
• Molecular Weight: 472.629
• Mol file: 1609652-86-9.mol

Synonyms:

Chemical Property of C₂₇H₃₇O₃PS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₃₇O₃PS

There total 4 articles about C₂₇H₃₇O₃PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl bromide (100-39-0) → C27H37O3PS (1609652-86-9) + C27H37O3PS

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium / tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique

1.2: 1 h / 67 °C / Inert atmosphere; Schlenk technique

2.1: sulfur; triethylamine / 20 h / 20 °C

3.1: chlorobenzene / 120 h / 130 °C / Inert atmosphere; Schlenk technique

With lithium; sulfur; triethylamine; In tetrahydrofuran; chlorobenzene; 3.1: |Diels-Alder Cycloaddition;

DOI:10.1039/c4cc00318g

Reference yield:

1-Benzyl-3,4-dimethylphosphole (38864-30-1) → C27H37O3PS (1609652-86-9) + C27H37O3PS

Guidance literature:

Multi-step reaction with 2 steps

1: sulfur; triethylamine / 20 h / 20 °C

2: chlorobenzene / 120 h / 130 °C / Inert atmosphere; Schlenk technique

With sulfur; triethylamine; In chlorobenzene; 2: |Diels-Alder Cycloaddition;

DOI:10.1039/c4cc00318g

Reference yield:

3,4-dimethyl-1-phenylphosphole (30540-36-4) → C27H37O3PS (1609652-86-9) + C27H37O3PS

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium / tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique

1.2: 1 h / 67 °C / Inert atmosphere; Schlenk technique

2.1: sulfur; triethylamine / 20 h / 20 °C

3.1: chlorobenzene / 120 h / 130 °C / Inert atmosphere; Schlenk technique

With lithium; sulfur; triethylamine; In tetrahydrofuran; chlorobenzene; 3.1: |Diels-Alder Cycloaddition;

DOI:10.1039/c4cc00318g

upstream raw materials:

benzyl bromide

(5R)-(L-menthyloxy)-2(5H)-furanone

3,4-dimethyl-1-phenylphosphole

1-Benzyl-3,4-dimethylphosphole

Downstream raw materials:

C₂₇H₃₇O₃P

C₂₇H₃₇O₃P