(1,3,3,5,5-pentafluorocyclotriphos(P(V))azen-1-yl)dicarbonylcyclopentadienyliron

Base Information

• Chemical Name: (1,3,3,5,5-pentafluorocyclotriphos(P(V))azen-1-yl)dicarbonylcyclopentadienyliron
• CAS No.: 84303-21-9
• Molecular Formula: C₇H₅F₅FeN₃O₂P₃
• Molecular Weight: 406.896

Synonyms:

Chemical Property of (1,3,3,5,5-pentafluorocyclotriphos(P(V))azen-1-yl)dicarbonylcyclopentadienyliron

Chemical Property:

Purity/Quality:

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Technology Process of (1,3,3,5,5-pentafluorocyclotriphos(P(V))azen-1-yl)dicarbonylcyclopentadienyliron

There total 1 articles about (1,3,3,5,5-pentafluorocyclotriphos(P(V))azen-1-yl)dicarbonylcyclopentadienyliron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

potassium cyclopentadienyldicarbonyliron(0) + hexafluorophosphazene (15599-91-4) → di(cyclopentadienideiron dicarbonyl) (38117-54-3) + 1,1-[μ-carbonyl-bis(carbonylcyclopentadienyliron)(Fe-Fe)]-3,3,5,5-tetrafluorocyclotriphosphazene (70538-16-8) + (1,3,3,5,5-pentafluorocyclotriphos(P(V))azen-1-yl)dicarbonylcyclopentadienyliron (84303-21-9)

Guidance literature:

In tetrahydrofuran; byproducts: N3P3F4(Fe(CO)2(C5H5))2; (N2), soln. of the KFe-complex added dropwise to a soln. of the org. compd., stirred at 25°C for 48 h, removed, dissolved in CH2Cl2; chromd. (silica gel), removed, dissolved (CH2Cl2), chromd. (silica gel/hexane slurry), Fe2(CO)4Cp2 eluted (CH2Cl2/hexane (1/5)), IR, MAS, eluted (CH2Cl2/hexane (1/1)), sublimed (25°C,0.1 torr), MAS, N3P3F4(Fe(CO)2Cp)2 eluted (CH2Cl2);

DOI:10.1021/ja00343a041

upstream raw materials:

hexafluorophosphazene

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