1,1-[μ-carbonyl-bis(carbonylcyclopentadienyliron)(Fe-Fe)]-3,3,5,5-tetrafluorocyclotriphosphazene

Base Information

Chemical Name:1,1-[μ-carbonyl-bis(carbonylcyclopentadienyliron)(Fe-Fe)]-3,3,5,5-tetrafluorocyclotriphosphazene
CAS No.:70538-16-8
Molecular Formula:C₁₃H₁₀F₄Fe₂N₃O₃P₃
Molecular Weight:536.85
Hs Code.:

Synonyms:

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Chemical Property of 1,1-[μ-carbonyl-bis(carbonylcyclopentadienyliron)(Fe-Fe)]-3,3,5,5-tetrafluorocyclotriphosphazene

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Technology Process of 1,1-[μ-carbonyl-bis(carbonylcyclopentadienyliron)(Fe-Fe)]-3,3,5,5-tetrafluorocyclotriphosphazene

There total 1 articles about 1,1-[μ-carbonyl-bis(carbonylcyclopentadienyliron)(Fe-Fe)]-3,3,5,5-tetrafluorocyclotriphosphazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: potassium cyclopentadienyldicarbonyliron⁽⁰⁾

: 15599-91-4
hexafluorophosphazene

: 38117-54-3
di(cyclopentadienideiron dicarbonyl)

: 70538-16-8
1,1-[μ-carbonyl-bis(carbonylcyclopentadienyliron)(Fe-Fe)]-3,3,5,5-tetrafluorocyclotriphosphazene

: 84303-21-9
(1,3,3,5,5-pentafluorocyclotriphos(P(V))azen-1-yl)dicarbonylcyclopentadienyliron

Guidance literature:: In tetrahydrofuran; byproducts: N3P3F4(Fe(CO)2(C5H5))2; (N2), soln. of the KFe-complex added dropwise to a soln. of the org. compd., stirred at 25°C for 48 h, removed, dissolved in CH2Cl2; chromd. (silica gel), removed, dissolved (CH2Cl2), chromd. (silica gel/hexane slurry), Fe2(CO)4Cp2 eluted (CH2Cl2/hexane (1/5)), IR, MAS, eluted (CH2Cl2/hexane (1/1)), sublimed (25°C,0.1 torr), MAS, N3P3F4(Fe(CO)2Cp)2 eluted (CH2Cl2);
DOI:10.1021/ja00343a041

Reference yield:

: 70538-16-8
1,1-[μ-carbonyl-bis(carbonylcyclopentadienyliron)(Fe-Fe)]-3,3,5,5-tetrafluorocyclotriphosphazene

: 38117-54-3
di(cyclopentadienideiron dicarbonyl)

Guidance literature:: With CO; In tetrahydrofuran; byproducts: N3P3F4(Fe(CO)2Cp)2; High Pressure; (N2), 1100 psi CO, 100°C for 18 h; cooled to room temp. under high CO pressure, chromd. on silica gel, eluted with CH2Cl2/hexane, IR, NMR;
DOI:10.1021/ja00343a041