methyl chrysenyl-6-acetate

Base Information

Chemical Name:methyl chrysenyl-6-acetate
CAS No.:859034-88-1
Molecular Formula:C₂₁H₁₆O₂
Molecular Weight:300.357
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl chrysenyl-6-acetate

Chemical Property:

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Technology Process of methyl chrysenyl-6-acetate

There total 7 articles about methyl chrysenyl-6-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 67-56-1
methanol

: 94688-59-2
chrysenyl-6-acetic acid

: 859034-88-1
methyl chrysenyl-6-acetate

Guidance literature:: With sulfuric acid; for 16h; Reflux;
DOI:10.1021/ol500154k

Reference yield:

: 218-01-9
chrysene

: 859034-88-1
methyl chrysenyl-6-acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: zirconium(IV) chloride / dichloromethane / 16 h / 25 °C

2.1: sodium iodide; hypophosphorous acid; acetic acid / water / 6 h / Reflux

2.2: 64 h / Reflux

3.1: sulfuric acid / 16 h / Reflux

With sulfuric acid; hypophosphorous acid; zirconium(IV) chloride; acetic acid; sodium iodide; In dichloromethane; water; 1.1: |Friedel-Crafts Acylation;
DOI:10.1021/ol500154k

Reference yield:

: 1573350-58-9
ethyl chrysenyl-6-glyoxylate

: 859034-88-1
methyl chrysenyl-6-acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium iodide; hypophosphorous acid; acetic acid / water / 6 h / Reflux

1.2: 64 h / Reflux

2.1: sulfuric acid / 16 h / Reflux

With sulfuric acid; hypophosphorous acid; acetic acid; sodium iodide; In water;
DOI:10.1021/ol500154k