Phosphorimidic acid, [2,2,2-trifluoro-1-phenyl-1-(2,2,3,3-tetrafluoropropoxy)ethyl]-, triethyl ester

Base Information

• Chemical Name: Phosphorimidic acid, [2,2,2-trifluoro-1-phenyl-1-(2,2,3,3-tetrafluoropropoxy)ethyl]-, triethyl ester
• CAS No.: 140476-54-6
• Molecular Formula: C17H23F7NO4P
• Molecular Weight: 469.337
• Mol file: 140476-54-6.mol

Synonyms:

Chemical Property of Phosphorimidic acid, [2,2,2-trifluoro-1-phenyl-1-(2,2,3,3-tetrafluoropropoxy)ethyl]-, triethyl ester

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Phosphorimidic acid, [2,2,2-trifluoro-1-phenyl-1-(2,2,3,3-tetrafluoropropoxy)ethyl]-, triethyl ester

There total 3 articles about Phosphorimidic acid, [2,2,2-trifluoro-1-phenyl-1-(2,2,3,3-tetrafluoropropoxy)ethyl]-, triethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.2%

2,2,3,3-tetrafluoropropanol (76-37-9) + triethoxyphosphazo-1-phenyl-1-chloro-2,2,2-trifluoroethane (124841-96-9) → triethoxy<<2,2,2-trifluoro-1-phenyl-1-(2,2,3,3-tetrafluoropropoxy)ethyl>imino>phosphorane (140476-54-6)

Guidance literature:

With triethylamine; In diethyl ether; at 20 ℃; for 2h;

Reference yield:

phenyltrifluoromethyl-N-chloroketimine (78488-59-2) → triethoxy<<2,2,2-trifluoro-1-phenyl-1-(2,2,3,3-tetrafluoropropoxy)ethyl>imino>phosphorane (140476-54-6)

Guidance literature:

Multi-step reaction with 2 steps

1: -20 °C

2: (C₂H₅)3N

With triethylamine;

Reference yield:

triethyl phosphite (122-52-1) → triethoxy<<2,2,2-trifluoro-1-phenyl-1-(2,2,3,3-tetrafluoropropoxy)ethyl>imino>phosphorane (140476-54-6)

Guidance literature:

Multi-step reaction with 2 steps

1: -20 °C

2: (C₂H₅)3N

With triethylamine;

upstream raw materials:

2,2,3,3-tetrafluoropropanol

triethoxyphosphazo-1-phenyl-1-chloro-2,2,2-trifluoroethane

phenyltrifluoromethyl-N-chloroketimine

triethyl phosphite

Refernces

• 1、 Markovskii, L. N.,Furin, G. G.,Shermolovich, Yu. G.. "POLYFLUORO-CONTAINING N,N-DICHLOROARYLAMIDES AND N-CHLORIMINO-2,5-CYCLOHEXADIENES". . p. 849 - 864. Retrieved 2007/10/02.