4-tert-butylphenyl 2-iodophenyl ketone

Base Information

• Chemical Name: 4-tert-butylphenyl 2-iodophenyl ketone
• CAS No.: 951889-75-1
• Molecular Formula: C₁₇H₁₇IO
• Molecular Weight: 364.226

Synonyms:

Chemical Property of 4-tert-butylphenyl 2-iodophenyl ketone

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

4-tert-Butyl-2'-iodobenzophenone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-tert-butylphenyl 2-iodophenyl ketone

There total 7 articles about 4-tert-butylphenyl 2-iodophenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butylbenzene (253185-03-4,253185-04-5) + 2-Iodobenzoyl chloride (609-67-6) → 4-tert-butylphenyl 2-iodophenyl ketone (951889-75-1)

Guidance literature:

With aluminum (III) chloride; at 0 - 20 ℃; for 16h;

DOI:10.1016/j.tet.2020.131864

Reference yield:

(2-aminophenyl)[4-(tert-butyl)phenyl]methanone (461694-82-6) → 4-tert-butylphenyl 2-iodophenyl ketone (951889-75-1)

Guidance literature:

With toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In water; acetonitrile; at 25 ℃; for 2h;

DOI:10.1021/acs.orglett.8b01812

Reference yield:

anthranilic acid N-methoxy-N-methylamide (133776-41-7) → 4-tert-butylphenyl 2-iodophenyl ketone (951889-75-1)

Guidance literature:

Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

2: toluene-4-sulfonic acid; sodium nitrite; potassium iodide / water; acetonitrile / 2 h / 25 °C

With n-butyllithium; toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In tetrahydrofuran; hexane; water; acetonitrile;

DOI:10.1021/acs.orglett.8b01812

upstream raw materials:

(2-aminophenyl)[4-(tert-butyl)phenyl]methanone

anthranilic acid N-methoxy-N-methylamide

1-bromo-4-tert-butylbenzene

isatoic anhydride

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