MnI₂(P(C₆H₅)3)2

Base Information

Chemical Name:MnI₂(P(C₆H₅)3)2
CAS No.:23661-58-7
Molecular Formula:C₃₆H₃₀I₂MnP₂
Molecular Weight:833.329
Hs Code.:

MnI<sub>2</sub>(P(C<sub>6</sub>H<sub>5</sub>)3)2

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of MnI₂(P(C₆H₅)3)2

Chemical Property:

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Technology Process of MnI₂(P(C₆H₅)3)2

There total 1 articles about MnI₂(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7439-96-5
manganese

: 6396-07-2
triphenylphosphine diiodide

: 7790-33-2
manganese(II) iodide

: 23661-58-7
MnI₂(P(C₆H₅)3)2

Guidance literature:: In diethyl ether; addn. of manganese powder to phosphorane soln. under strictly anaerobic and anhydrous conditions; pptn. after 4d; isolation; drying (vac.); concentrating of filtrate to half the volume; further isolation of complex; sealing products in ampoules in a flame;
DOI:10.1039/DT9930000371

Reference yield:

: 23661-58-7
MnI₂(P(C₆H₅)3)2

: 119072-55-8,7188-38-7
tert-butylisonitrile

: {MnI₂(P(C₆H₅)3)(CNC(CH₃)3)2}2

Guidance literature:: In pentane; under Ar, Mn-compd. added to n-pentane, t-BuNC added, stirred for 72 h; crystals collected, washed with n-pentane, dried in vac., elem. anal.;
DOI:10.1016/S0020-1693(00)92344-2

Reference yield:

: 23661-58-7
MnI₂(P(C₆H₅)3)2

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 144391-67-3
Mn(CNC(CH₃)3)6⁽¹⁺⁾*MnI₃(P(C₆H₅)3)^(1-) = {Mn(CNC(CH₃)3)6}{MnI₃(P(C₆H₅)3)}

: 144391-67-3
Mn(CNC(CH₃)3)5(P(C₆H₅)3)⁽¹⁺⁾*MnI₃(CNC(CH₃)3)^(1-) = {Mn(CNC(CH₃)3)5(P(C₆H₅)3)}{MnI₃(CNC(CH₃)3)}

Guidance literature:: In toluene; under Ar, excess of t-BuNC added to a suspn. of Mn-compd. in toluene, stirred for 48 h; filtered, filtrate slowly evapd., fractional crystn., elem. anal.;
DOI:10.1016/S0020-1693(00)92344-2